(S)-3-(甲基氨基)-1-苯丙醇合成路线 （共 40 条）
反应条件
hydrogen; potassium carbonate; [Rh{(SC,RP)-duanphos}(norbornadiene)]SbF6 in methanol T=20°C; P=7500.6 Torr; 12 h;
参考文献
Liu, Duan; Gao, Wenzhong; Wang, Chunjiang; Zhang, Xumu
Angewandte Chemie - International Edition, 2005 , vol. 44, # 11 p. 1687 - 1689
反应条件
lithium hydroxide; hydrogen; RuCl2 in isopropyl alcohol T=30°C; P=22502.3 Torr; 18 h;
参考文献
EP1411045 A1, ;
Page 19 ;
反应条件
lithium aluminium tetrahydride in diethyl ether
参考文献
Kumar, Ashok; Ner, Dilip H.; Dike, Suneel Y.
Tetrahedron Letters, 1991 , vol. 32, # 16 p. 1901 - 1904
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran T=20°C; 3 h;
参考文献
Tetrahedron Asymmetry, , vol. 24, # 15-16 p. 913 - 918
反应条件
in tetrahydrofuran; water T=65°C; 3 h;
参考文献
Gao, Y.; Sharpless, K. B.
Journal of Organic Chemistry, 1988 , vol. 53, # 17 p. 4081 - 4084
反应条件
1: 90 percent / NaI / acetone / Heating 2: 86 percent / tetrahydrofuran; H2O / Ambient temperature View Scheme
参考文献
Tetrahedron, , vol. 48, # 33 p. 6769 - 6776
反应条件
1: 3-hydroxy-3-phenylpropyl 4-toluenesulfonate With 3 A molecular sieve; oxygen; (-)-sparteine; palladium diacetate in toluene T=80°C; P=760 Torr; 36 h; 2: methylamine With water in tetrahydrofuran T=65°C;
参考文献
Tetrahedron Letters, , vol. 43, # 31 p. 5435 - 5436
反应条件
1: HCl / ethanol / 110 °C 2: 90 percent / hydrogen; K2CO3 / [Rh{(SC,RP)-duanphos}(norbornadiene)]SbF6 / methanol / 12 h / 20 °C / 7500.6 Torr View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 44, # 11 p. 1687 - 1689
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 5.5 h; Heating;
参考文献
Caspi, Daniel D.; Ebner, David C.; Bagdanoff, Jeffrey T.; Stoltz, Brian M.
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 2-3 p. 185 - 189
反应条件
in tetrahydrofuran; water Ambient temperature;
参考文献
Chenevert, Robert; Fortier, Genevieve
Chemistry Letters, 1991 , p. 1603 - 1606
Title/Abstract Full Text Show Details
Chenevert, Robert; Fortier, Genevieve; Rhlid, Rachid Bel
Tetrahedron, 1992 , vol. 48, # 33 p. 6769 - 6776
