1: With ozone in methanol
T=-50°C; 0.166667 h;
2: With dimethylsulfide in methanol
T=20°C; 1 h;
参考文献
Brimble, Margaret A.; Flowers, Christopher L.; Hutchinson, James K.; Robinson, James E.; Sidford, Matthew
Tetrahedron, 2005 , vol. 61, # 42 p. 10036 - 10047
1.1: 96 percent / imidazole; 4-dimethylaminopyridine / CH2Cl2 / 3 h / 0 °C
2.1: ozone / methanol / 0.17 h / -50 °C
2.2: 95 percent / dimethyl sulfide / methanol / 1 h / 20 °C
View Scheme
参考文献
Brimble, Margaret A.; Flowers, Christopher L.; Hutchinson, James K.; Robinson, James E.; Sidford, Matthew
Tetrahedron, 2005 , vol. 61, # 42 p. 10036 - 10047
