(1S,5R)-5-异丙基-2-亚甲基-3-环己烯-1-醇合成路线 (共 3 条)
反应条件
sulfuric acid; sodium perchlorate in tetrahydrofuran; water T=22°C; electrolytic oxidation, graphite electrodes; Title compound not separated from byproducts;
参考文献
Montiel, V.; Lopez, M.; Aldaz, A.; Barba, F.
Synthetic Communications, 1987 , vol. 17, # 8 p. 993 - 996
反应条件
water in tetrahydrofuran T=24°C; anodic oxidation on graphite electrodes in neutral and basic media; Product distributionMechanism;
参考文献
Montiel, Vicente; Lopez-Segura, Marcelo; Duo, Roberto; Aldaz, Antonio; Barba, Fructuoso
Journal of Chemical Research, Miniprint, 1987 , # 9 p. 2536 - 2547
反应条件
(i) MCPBA, aq. NaHCO3, CH2Cl2, (ii) LDA, Et2O, hexane; Multistep reaction;
参考文献
Escher; Keller; Willhalm
Helvetica Chimica Acta, 1979 , vol. 62, # 7 p. 2061 - 2072