4,4'-二氯二苯二硫醚合成路线 (共 295 条)
反应条件
1: conc. H2SO4 / methanol / 5 h / Heating 2: 0.14 g / 70percent H2SO4 / 2 h / 100 °C / r.t., overnight View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 25, p. 321 - 326
反应条件
4,4'-bis(trimethylaminomethyl)-2,2'-bipyridine dihydrobromide; FeCl3·6H2O; potassium hydroxide 24 h; Reflux;
参考文献
Green Chemistry, , vol. 11, # 3 p. 326 - 329
反应条件
sodium ethanolate in ethanol 4 h; Heating;
参考文献
Journal of Heterocyclic Chemistry, , vol. 25, p. 321 - 326
反应条件
in cyclohexane T=23°C; Kinetics;
参考文献
Journal of the American Chemical Society, , vol. 102, # 2 p. 698 - 701
反应条件
sulfur(2+); N(Et)4ClO4; triethylamine; trichloroacetic acid in dichloromethane 2 h; Ambient temperatureelectrochemical generation of S(2+) from carbon-sulfur anode before addition of thiol;
参考文献
Bulletin de la Societe Chimique de France, , vol. 133, # 3 p. 273 - 281
反应条件
T=500°C; P=0.001 - 0.1 Torr; Further byproducts given;
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 20 p. 3345 - 3348
反应条件
sodium hydride in N,N-dimethyl-formamide T=20°C; Substitution; Reduction; 5 h; Product distribution; Further Variations:ReagentsSolventsratio of reagents;
参考文献
Journal of Fluorine Chemistry, , vol. 102, # 1-2 p. 105 - 109
反应条件
acetic acid T=130 - 135°C;
参考文献
Journal of the Chemical Society, , p. 815,816
反应条件
acetic acid T=130 - 135°C;
参考文献
Journal of the Chemical Society, , p. 815,816
反应条件
acetic acid T=100°C;
参考文献
Journal of the Chemical Society, , p. 815,816