4,4'-二氯二苯二硫醚合成路线 (共 295 条)
反应条件
1-n-butyl-3-methylimidazolium chloride T=90°C; 8 h;
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 186, # 1 p. 31 - 37
反应条件
sulfuric acid in carbon disulfide 40 h; Ambient temperature;
参考文献
Phosphorus and Sulfur and the Related Elements, , vol. 29, p. 265 - 270
反应条件
in tetrahydrofuran; diethyl ether; benzene 12 h; Ambient temperature;
参考文献
Liebigs Annalen der Chemie, , # 3 p. 406 - 419
反应条件
sodium hydroxide; tetra-(n-butyl)ammonium iodide; trifluoroacetic anhydride 1.) CH2Cl2, 22h, room temp., 2.) room temp.; Yield given. Multistep reaction;
参考文献
Tetrahedron Letters, , vol. 21, p. 1235 - 1238
反应条件
sodium tetrahydroborate in tetrahydrofuran 10 h; Heating;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 35, # 5 p. 1770 - 1776
反应条件
piperidine in ethanol 16 h; Heating;
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 24, p. 940 - 947
反应条件
ammonium cerium(IV) nitrate in water; acetic acid T=25 - 45°C; ΔH(excit.), ΔS(excit.); KineticsThermodynamic data;
参考文献
Tetrahedron, , vol. 50, # 48 p. 13731 - 13738
反应条件
antimony trichloride in dichloromethane; toluene Ambient temperature; Further byproducts given. Title compound not separated from byproducts;
参考文献
Journal of Chemical Research, Miniprint, , # 12 p. 3123 - 3143
反应条件
T=500°C; P=0.001 - 0.1 Torr; Further byproducts given;
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 20 p. 3345 - 3348
反应条件
in N,N-dimethyl-formamide 4 h; Photolysis;
参考文献
Journal of the Chemical Society, Perkin Transactions 2, , # 9 p. 1557 - 1565