4,4'-二氯二苯二硫醚合成路线 (共 295 条)
反应条件
tetra-(n-butyl)ammonium iodide in benzene T=20°C; 18 h;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 19, # 10 p. 1875 - 1880
Zhurnal Organicheskoi Khimii, , vol. 19, # 10 p. 2158 - 2163
反应条件
silver nitrate in ethanol; N,N-dimethyl-formamide T=110°C; 6 h;
参考文献
Gogoi, Prasanta; Gogoi, Sandhya R.; Kalita, Mukul; Barman, Pranjit
Synlett, 2013 , vol. 24, # 7 art. no. ST-2012-D0136-L, p. 873 - 877
反应条件
aluminium trichloride; zinc in water; N,N-dimethyl-formamide T=65°C; 8 h;
参考文献
Lakouraj; Movassagh; Fadaei
Synthetic Communications, 2002 , vol. 32, # 8 p. 1237 - 1242
反应条件
KOH adsorbed on neutral alumina in neat (no solvent) 0.25 h; Milling; Reagent/catalystTime;
参考文献
Mukherjee, Nirmalya; Chatterjee, Tanmay; Ranu, Brindaban C.
Journal of Organic Chemistry, 2013 , vol. 78, # 21 p. 11110 - 11114
反应条件
antimony(V) pentachloride in dichloromethane T=25°C; 2 h;
参考文献
Takeuchi, Hiroshi; Hiyama, Takehiro; Kamai, Noriyoshi; Oya, Hiromi
Journal of the Chemical Society. Perkin Transactions 2, 1997 , # 11 p. 2301 - 2305
反应条件
iron; potassium carbonate in dimethyl sulfoxide; N,N-dimethyl-formamide T=120°C; 18 h; Inert atmosphere;
参考文献
Li, Yaming; Nie, Caiping; Wang, Huifeng; Li, Xiaoying; Verpoort, Francis; Duan, Chunying
European Journal of Organic Chemistry, 2011 , # 36 p. 7331 - 7338
反应条件
copper(I) sulphide; iron; potassium carbonate; dimethyl sulfoxide T=110°C; 18 h; Inert atmosphere; chemoselective reaction;
参考文献
Wang, Huifeng; Jiang, Linlin; Chen, Tao; Li, Yarning
European Journal of Organic Chemistry, 2010 , # 12 p. 2324 - 2329
反应条件
in acetonitrile T=80°C; 12 h; dark; Yield given. Yields of byproduct given;
参考文献
Oae, Shigeru; Nagata, Toshiyuki; Yoshimura, Toshiaki; Fujimori, Ken
Tetrahedron Letters, 1982 , vol. 23, # 31 p. 3189 - 3192
反应条件
sodium formaldehyde sulfoxylate dihydrate; potassium carbonate in N,N-dimethyl-formamide T=20°C; 0.0833333 h; regioselective reaction;
参考文献
Guo, Wenxue; Chen, Jiuxi; Wu, Dengze; Ding, Jinchang; Chen, Fan; Wu, Huayue
Tetrahedron, 2009 , vol. 65, # 27 p. 5240 - 5243
反应条件
oxygen; copper (II) acetate monohydrate; caesium carbonate in acetonitrile T=130°C; 24 h; Sealed tube;
参考文献
Zou, Liang-Hua; Priebbenow, Daniel L.; Wang, Long; Mottweiler, Jakob; Bolm, Carsten
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 13 p. 2558 - 2563