4,4'-二氯二苯二硫醚合成路线 (共 295 条)
反应条件
water; hydroxymethanesulfinic acid sodium salt; potassium carbonate in N,N-dimethyl-formamide 0.25 h;
参考文献
Tang, Ri-Yuan; Zhong, Ping; Lin, Qiu-Lian
Synthesis, 2007 , # 1 p. 85 - 91
反应条件
bis-[(trifluoroacetoxy)iodo]benzene 3 h; Heating;
参考文献
Xia; Chen
Synthetic Communications, 1997 , vol. 27, # 8 p. 1321 - 1326
反应条件
2,4-di-Nitrobenzene in benzene T=20°C; Addition; 24 h; Irradiation; Further byproducts given. Title compound not separated from byproducts;
参考文献
Leardini, Rino; Nanni, Daniele; Zanardi, Giuseppe
Journal of Organic Chemistry, 2000 , vol. 65, # 9 p. 2763 - 2772
反应条件
24 h; HeatingIrradiation; Product distributionMechanism;
参考文献
Martynov, A. V.; Mirskova, A. N.; Voronkov, M. G.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, # 1 p. 20 - 25
Zhurnal Organicheskoi Khimii, 1984 , vol. l, # 1 p. 23 - 29
反应条件
18-crown-6 ether 1.) pyridine, 25 deg C, 0.5 h; 2.) H2O-MeOH, overnight, room temp.; Yield given. Multistep reaction;
参考文献
Tetrahedron, , vol. 37, p. 37 - 44
反应条件
chloro-trimethyl-silane; potassium nitrate in dichloromethane T=50°C; 8 h;
参考文献
Journal of Organic Chemistry, , vol. 72, # 15 p. 5847 - 5850
反应条件
in tetrahydrofuran T=23°C; Rate constant;
参考文献
Tagaya, Hideyuki; Aruga, Tamotsu; Ito, Osamu; Matsuda, Minoru
Journal of the American Chemical Society, 1981 , vol. 103, # 18 p. 5484 - 5489
反应条件
dihydrogen peroxide; trichlorophosphate in water T=80°C; 1 h; Micellar solution;
参考文献
Bahrami, Kiumars; Khodaei, Mohammad M.; Abbasi, Jamshid
Synthesis, 2012 , vol. 2012, # 2 p. 316 - 322
参考文献
Wang, Z. Y.; Bonanno, G.; Hay, A. S.
Journal of Organic Chemistry, 1992 , vol. 57, # 9 p. 2751 - 2753
反应条件
bis-[(trifluoroacetoxy)iodo]benzene 7 h; Heating;
参考文献
Xia; Chen
Synthetic Communications, 1997 , vol. 27, # 8 p. 1321 - 1326