4,4'-二氯二苯二硫醚合成路线 (共 295 条)
反应条件
in tetrahydrofuran T=22.4°C; Rate constant;
参考文献
Tagaya, Hideyuki; Aruga, Tamotsu; Ito, Osamu; Matsuda, Minoru
Journal of the American Chemical Society, 1981 , vol. 103, # 18 p. 5484 - 5489
反应条件
water; 1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate) in acetonitrile 3 h; Reflux;
参考文献
Kirihara, Masayuki; Naito, Sayuri; Nishimura, Yuki; Ishizuka, Yuki; Iwai, Toshiaki; Takeuchi, Haruka; Ogata, Tomomi; Hanai, Honoka; Kinoshita, Yukari; Kishida, Mari; Yamazaki, Kento; Noguchi, Takuya; Yamashoji, Shiro
Tetrahedron, 2014 , vol. 70, # 14 p. 2464 - 2471
反应条件
water; 1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate) in acetonitrile T=20°C; 0.333333 h;
参考文献
Kirihara, Masayuki; Naito, Sayuri; Nishimura, Yuki; Ishizuka, Yuki; Iwai, Toshiaki; Takeuchi, Haruka; Ogata, Tomomi; Hanai, Honoka; Kinoshita, Yukari; Kishida, Mari; Yamazaki, Kento; Noguchi, Takuya; Yamashoji, Shiro
Tetrahedron, 2014 , vol. 70, # 14 p. 2464 - 2471
反应条件
T=30°C; 28 h; Irradiation; Product distributionMechanism;
参考文献
Martynov, A. V.; Mirskova, A. N.; Voronkov, M. G.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, # 1 p. 20 - 25
Zhurnal Organicheskoi Khimii, 1984 , vol. l, # 1 p. 23 - 29
反应条件
in benzene Irradiation (UV/VIS); stirred at 35°C for 90 min;
参考文献
Mirzaei, Farzad; Han, Li-Biao; Tanaka, Masato
Chemical Communications, 2000 , # 8 p. 657 - 658
反应条件
sulfur; cis-DPPEthylene; [Rh(H)(PEt3)3] in acetone T=20°C; 0.0833333 h;
参考文献
Arisawa, Mieko; Tanaka, Ken; Yamaguchi, Masahiko
Tetrahedron Letters, 2005 , vol. 46, # 28 p. 4797 - 4800
反应条件
potassium hydroxide; potassium chloride in isopropyl alcohol T=25°C; various carbanions and disubstituted diaryl disulfides investigated; Rate constant;
参考文献
Gilbert, H. F.
Journal of the American Chemical Society, 1980 , vol. 102, # 23 p. 7059 - 7065
反应条件
2,4-di-Nitrobenzene in benzene T=20°C; Addition; 24 h; Irradiation; Further byproducts given;
参考文献
Leardini, Rino; Nanni, Daniele; Zanardi, Giuseppe
Journal of Organic Chemistry, 2000 , vol. 65, # 9 p. 2763 - 2772
反应条件
copper(l) iodide; zinc in glycerol T=110°C; 24 h; Inert atmosphere; Overall yield = 60 percent; Overall yield = 0.088 g;
参考文献
Goncalves, Loren C.C.; Lima, David B.; Borba, Pedro M.Y.; Perin, Gelson; Alves, Diego; Jacob, Raquel G.; Lenardao, Eder J.
Tetrahedron Letters, 2013 , vol. 54, # 26 p. 3475 - 3480
反应条件
1,10-phenanthroline; oxygen; anhydrous copper acetate in dimethyl sulfoxide T=100°C; 7 h; Air atmosphere;
参考文献
Yasuike, Shuji; Nishioka, Motokazu; Kakusawa, Naoki; Kurita, Jyoji
Tetrahedron Letters, 2011 , vol. 52, # 48 p. 6403 - 6406