4,4'-二氯二苯二硫醚合成路线 （共 295 条）
反应条件
tetrachloromethane; sodium hydroxide in water; N,N-dimethyl-formamide
参考文献
Wenschuh, Eberhard; Hesselbarth, Frank
Phosphorus, Sulfur and Silicon and the Related Elements, 1991 , vol. 59, # 1-4 p. 133 - 136
反应条件
1: 4,4'-dichlorodiphenyl disulfide With aluminium trichloride; zinc in N,N-dimethyl-formamide T=65°C; 2: methyloxirane in N,N-dimethyl-formamide T=65°C; 3 h;
参考文献
Movassagh; Sobhani; Kheirdoush; Fadaei
Synthetic Communications, 2003 , vol. 33, # 18 p. 3103 - 3108
反应条件
1: 4,4'-dichlorodiphenyl disulfide With bis(cyclopentadienyl)titanium dichloride; zinc in tetrahydrofuran T=20°C; Inert atmosphere; 2: ethyl acrylate in tetrahydrofuran T=20°C; 3.5 h; Inert atmosphere;
参考文献
Xu, Xiao Bo; Yin, Xian Hong; Zhu, Yu Yang; Xu, Xin Hua; Luo, Tao; Li, Yin Hui; Lu, Xiong; Shao, Ling Ling; Pan, Jian Gao; Yang, Rong Hua
Journal of Chemical Research, 2009 , # 12 p. 750 - 752
反应条件
aluminium trichloride; zinc in water; N,N-dimethyl-formamide T=65°C; 6 h;
参考文献
Lakouraj; Movassagh; Fadaei
Synthetic Communications, 2002 , vol. 32, # 8 p. 1237 - 1242
反应条件
iron; potassium carbonate in dimethyl sulfoxide; N,N-dimethyl-formamide T=120°C; 18 h; Inert atmosphere;
参考文献
Li, Yaming; Nie, Caiping; Wang, Huifeng; Li, Xiaoying; Verpoort, Francis; Duan, Chunying
European Journal of Organic Chemistry, 2011 , # 36 p. 7331 - 7338
反应条件
1.1: n-butyllithium / tetrahydrofuran; hexane / 0.17 h / -78 °C 1.2: tetrahydrofuran; hexane / -78 °C 2.1: 3-chloroperoxybenzoic acid / CH2Cl2 3.1: 30 percent / silver(I) carbonate; tricyclohexylphosphine / palladium(II) acetate / dimethylformamide / 72 h / 110 °C View Scheme
参考文献
Ruano, Jose Luis Garcia; Aleman, Jose; Paredes, Cristina Garcia
Organic Letters, 2006 , vol. 8, # 13 p. 2683 - 2686
反应条件
N-bromosuccinmide in acetonitrile T=25°C; 15 h;
参考文献
Liang, Gaigai; Liu, Miaochang; Chen, Jiuxi; Ding, Jinchang; Gao, Wenxia; Wu, Huayue
Chinese Journal of Chemistry, 2012 , vol. 30, # 7 p. 1611 - 1616
反应条件
1: 1.) LDA / 1.) THF, -70 deg C, 1 h, 2.) THF, -70 deg C, 1 h 2: HCl (conc.) / 2 h / Ambient temperature View Scheme
参考文献
Tanaka, Hiromichi; Takashima, Hideaki; Ubasawa, Masaru; Sekiya, Kouichi; Nitta, Iasei; et al.
Journal of Medicinal Chemistry, 1992 , vol. 35, # 2 p. 337 - 345
反应条件
triphenylphosphine in benzene 24.5 h; Heatingvar. time, var. ratio of reaction partners, other reaction partners - various diaryl disulfides, tributylamine; Product distributionMechanism;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 57, # 1 p. 232 - 236
反应条件
1: 4,4'-dichlorodiphenyl disulfide With triphenylphosphine in 1,4-dioxane; water
T=100°C;
2: para-nitrophenyl mercaptan With iodine; potassium iodide in dichloromethane
10 h;
参考文献
Sudharsanam, Ramanathan; Chandrasekarana, Srinivasan; Das Kumar, Puspendu
Journal of Materials Chemistry, 2002 , vol. 12, # 10 p. 2904 - 2908
