4,4'-二氯二苯二硫醚合成路线 （共 295 条）
反应条件
sulfur in ammonia
T=20°C; 2 h; variation of temperature and amount of raegent; MechanismProduct distribution;
参考文献
Sato, Ryu; Chiba, Shuji; Saito, Nobushige; Sato, Mikiya; Saito, Minoru
Phosphorus and Sulfur and the Related Elements, 1984 , vol. 19, p. 205 - 212
反应条件
hydroxymethanesulfinic acid sodium salt; potassium carbonate in N,N-dimethyl-formamide
T=20°C; 0.166667 h; chemoselective reaction;
参考文献
Guo, Wenxue; Lv, Guangshu; Chen, Jiuxi; Gao, Wenxia; Ding, Jinchang; Wu, Huayue
Tetrahedron, 2010 , vol. 66, # 13 p. 2297 - 2300
反应条件
water; 1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate) in acetonitrile
T=20°C; 0.333333 h;
参考文献
Kirihara, Masayuki; Naito, Sayuri; Nishimura, Yuki; Ishizuka, Yuki; Iwai, Toshiaki; Takeuchi, Haruka; Ogata, Tomomi; Hanai, Honoka; Kinoshita, Yukari; Kishida, Mari; Yamazaki, Kento; Noguchi, Takuya; Yamashoji, Shiro
Tetrahedron, 2014 , vol. 70, # 14 p. 2464 - 2471
反应条件
ammonium cerium (IV) nitrate; iodine; oxygen in poly(ethylene glycol) 400; water
T=60°C; 1.25 h; chemoselective reaction;
参考文献
Cai, Ming-Tiao; Lv, Guang-Shu; Chen, Jiu-Xi; Gao, Wen-Xia; Ding, Jin-Chang; Wu, Hua-Yue
Chemistry Letters, 2010 , vol. 39, # 4 p. 368 - 369
反应条件
N-bromosuccinmide in acetonitrile
T=25°C; 15 h;
参考文献
Liang, Gaigai; Liu, Miaochang; Chen, Jiuxi; Ding, Jinchang; Gao, Wenxia; Wu, Huayue
Chinese Journal of Chemistry, 2012 , vol. 30, # 7 p. 1611 - 1616
反应条件
1: 83 percent / Na2HPO4; Na2S2O4 / dimethylformamide; H2O / 2.5 h / 20 °C / 9000.9 Torr
2: 98 percent / trichloroisocyanuric acid; [Bmim]BF4; H2O / 1 h / 20 °C
View Scheme
参考文献
Tang, Ri-Yuan; Zhong, Ping; Lin, Qiu-Lian
Journal of Fluorine Chemistry, 2007 , vol. 128, # 6 p. 636 - 640
反应条件
2,4-di-Nitrobenzene in benzene
T=20°C; Addition; 24 h; Irradiation; Further byproducts given. Title compound not separated from byproducts;
参考文献
Leardini, Rino; Nanni, Daniele; Zanardi, Giuseppe
Journal of Organic Chemistry, 2000 , vol. 65, # 9 p. 2763 - 2772
反应条件
1: Cl2 / CCl4 / 0 °C
2: benzene; pyridine / 0.67 h / Ambient temperature
View Scheme
参考文献
Baldwin, Jack E.; Norris, Robert K.
Journal of Organic Chemistry, 1981 , vol. 46, # 4 p. 697 - 703
反应条件
T=30°C; 28 h; Irradiation; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Martynov, A. V.; Mirskova, A. N.; Voronkov, M. G.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, # 1 p. 20 - 25
Zhurnal Organicheskoi Khimii, 1984 , vol. l, # 1 p. 23 - 29
反应条件
T=30°C; 28 h; Irradiation; Product distributionMechanism;
参考文献
Martynov, A. V.; Mirskova, A. N.; Voronkov, M. G.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, # 1 p. 20 - 25
Zhurnal Organicheskoi Khimii, 1984 , vol. l, # 1 p. 23 - 29
