4,4'-二氯二苯二硫醚合成路线 （共 295 条）
反应条件
hydrogenchloride; zinc in water
T=20°C; 0.333333 h; Ionic liquidInert atmosphere;
参考文献
Narayanaperumal, Senthil; Alberto, Eduardo E.; Gul, Kashif; Kawasoko, Cristiane Yuriko; Dornelles, Luciano; Rodrigues, Oscar E.D.; Braga, Antonio Luiz
Tetrahedron, 2011 , vol. 67, # 25 p. 4723 - 4730
反应条件
water; hydroxymethanesulfinic acid sodium salt; potassium carbonate in N,N-dimethyl-formamide
0.25 h;
参考文献
Tang, Ri-Yuan; Zhong, Ping; Lin, Qiu-Lian
Synthesis, 2007 , # 1 p. 85 - 91
反应条件
aluminium trichloride; zinc in water; acetonitrile
T=65°C; 4 h;
参考文献
Movassagh, Barahman; Mossadegh, Amir
Synthetic Communications, 2004 , vol. 34, # 9 p. 1685 - 1690
反应条件
iodine in 1-methyl-pyrrolidin-2-one
T=130°C; 0.666667 h; Sealed tubeMicrowave irradiation;
参考文献
Hu, Bolun; Sun, Leilei; Tang, Riyuan; Hu, Huanan
Chinese Journal of Chemistry, 2012 , vol. 30, # 10 p. 2556 - 2562,7
反应条件
in chloroform
T=20°C; 0.5 h;
参考文献
Mukaiyama, Teruaki; Ikegai, Kazuhiro
Chemistry Letters, 2004 , vol. 33, # 11 p. 1522 - 1523
反应条件
in acetonitrile
T=80°C; 12 h; dark; Yield given. Yields of byproduct given;
参考文献
Oae, Shigeru; Nagata, Toshiyuki; Yoshimura, Toshiaki; Fujimori, Ken
Tetrahedron Letters, 1982 , vol. 23, # 31 p. 3189 - 3192
反应条件
air; nitrogen(II) oxide in acetonitrile
T=20°C;
参考文献
Tsutsumi; Itoh; Ohsawa
Chemical and Pharmaceutical Bulletin, 2000 , vol. 48, # 10 p. 1524 - 1528
反应条件
hydroxymethanesulfinic acid sodium salt; potassium carbonate in N,N-dimethyl-formamide
T=20°C; 0.166667 h; chemoselective reaction;
参考文献
Guo, Wenxue; Lv, Guangshu; Chen, Jiuxi; Gao, Wenxia; Ding, Jinchang; Wu, Huayue
Tetrahedron, 2010 , vol. 66, # 13 p. 2297 - 2300
反应条件
aluminium trichloride; zinc in water; acetonitrile
T=65°C; 8 h;
参考文献
Movassagh, Barahman; Mossadegh, Amir
Synthetic Communications, 2004 , vol. 34, # 9 p. 1685 - 1690
反应条件
1: 4,4'-dichlorodiphenyl disulfide With aluminium trichloride; zinc in water; N,N-dimethyl-formamide
T=65°C; S-S bond cleavage;
2: 1-bromo-hexane in water; N,N-dimethyl-formamide
T=65°C; Substitution; 18 h;
参考文献
Movassagh; Lakouraj; Fadaei
Journal of Chemical Research - Part S, 2000 , # 7 p. 350 - 351
