4,4'-二氯二苯二硫醚合成路线 (共 295 条)
反应条件
potassium carbonate; boron trifluoride diethyl etherate in dichloromethane 0.0333333 h; Ambient temperature;
参考文献
Benati, L.; Montevecchi, P. C.; Spagnolo, P.
Tetrahedron Letters, 1986 , vol. 27, # 15 p. 1739 - 1742
反应条件
in chloroform 0.05 h; Microwave irradiation;
参考文献
Kutuk, Halil; Turkoz, Nalan
Phosphorus, Sulfur and Silicon and the Related Elements, 2011 , vol. 186, # 7 p. 1515 - 1522
反应条件
sulfur; copper(l) iodide; lithium hydroxide hydrate in N,N-dimethyl-formamide T=100°C; 24 h; Inert atmosphere;
参考文献
Organometallics, , vol. 32, # 19 p. 5514 - 5522
反应条件
para-dinitrobenzene; 2-nitro-2-thiocyanatopropane in dimethyl sulfoxide 2 h; Irradiation;
参考文献
Tetrahedron Letters, , vol. 24, # 24 p. 2517 - 2520
反应条件
sulfuric acid T=100°C; 2 h; r.t., overnight;
参考文献
Journal of Heterocyclic Chemistry, , vol. 25, p. 321 - 326
反应条件
methanesulfonic acid T=75°C; 6 h;
参考文献
Tetrahedron, , vol. 49, # 4 p. 939 - 946
反应条件
pyridine; dimethylsulfide in nitromethane
参考文献
Bodrikov, I. V.; Shebelova, I. Yu.; Korchagina, D. V.; Gatilov, Yu. V.; Tishkov, K. N.; et al.
Journal of Organic Chemistry USSR (English Translation), 1992 , vol. 28, # 10 p. 1644 - 1650
Zhurnal Organicheskoi Khimii, 1992 , vol. 28, # 10 p. 2054 - 2062
反应条件
tin(IV) chloride T=0°C; Further byproducts given;
参考文献
Journal of Chemical Research, Miniprint, , # 12 p. 3123 - 3143
反应条件
lithium perchlorate in nitromethane T=20°C; Further byproducts given;
参考文献
Russian Journal of Organic Chemistry, , vol. 31, # 7 p. 943 - 951
Zhurnal Organicheskoi Khimii, , vol. 31, # 7 p. 1018 - 1026
反应条件
hydridotetrakis(triphenylphosphine)rhodium (Ph3P)4RhH; 1,2-bis-(diphenylphosphino)ethane in N,N-dimethyl acetamide T=20°C; 3 h; Inert atmosphere;
参考文献
Tetrahedron Letters, , vol. 53, # 43 p. 5729 - 5732