3-Boc-6-氧杂-3-氮杂二环[3.1.0]己烷合成路线 （共 17 条）
反应条件
Oxonereg;; ethylenediaminetetraacetic acid in various solvent(s)
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 15, # 21 p. 4770 - 4773
反应条件
1: in methanol T=0 - 20°C; 24 h; 2: With 3-chloro-benzenecarboperoxoic acid in dichloromethane T=0 - 20°C; 48 h;
参考文献
WO2005/26111 A2, ;
Page/Page column 15 ;
WO 2005/026111 A2
反应条件
sodium hydroxide in tetrahydrofuran T=20°C; 2 h;
参考文献
WO2013/138210 A1, ;
Paragraph 0184 ;
反应条件
sodium hydrogencarbonate; sodium thiosulfate in chloroform; water; ethyl acetate; toluene
反应条件
1: methanol / 15 h / 20 °C 2: m-CPBA / CH2Cl2 / 48 h / 20 °C View Scheme
参考文献
Tetrahedron Asymmetry, , vol. 12, # 21 p. 2989 - 2997
反应条件
1: 92 percent / Cl2(PCy)3Ru=CH-Ph / benzene 2: 100 percent / potassium peroxymonosulfate; EDTA / various solvent(s) View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 15, # 21 p. 4770 - 4773
反应条件
1: 60 percent / NaH / dimethylformamide / 5.67 h / 20 - 50 °C 2: m-CPBA / CH2Cl2 / 48 h / 20 °C View Scheme
参考文献
Tetrahedron Asymmetry, , vol. 12, # 21 p. 2989 - 2997
反应条件
in diethyl ether; hexane T=-78 - 25°C; 2 h;
参考文献
Hodgson, David M.; Miles, Timothy J.; Witherington, Jason
Tetrahedron, 2003 , vol. 59, # 49 p. 9729 - 9742
反应条件
in diethyl ether; hexane T=-78 - 25°C; 2 h;
参考文献
Hodgson, David M.; Miles, Timothy J.; Witherington, Jason
Tetrahedron, 2003 , vol. 59, # 49 p. 9729 - 9742
反应条件
in diethyl ether; pentane T=-78 - 25°C; 2 h;
参考文献
Hodgson, David M.; Miles, Timothy J.; Witherington, Jason
Tetrahedron, 2003 , vol. 59, # 49 p. 9729 - 9742
