(R)-3-苄氧基肉豆蔻酸甲酯合成路线 （共 13 条）
反应条件
1: 1) 2 eq. dicyclohexylborane; 2) NaOH, H2O2 / 1) THF, 0 deg C; 2) 40-50 deg C
2: HCl / 2 h / Ambient temperature
3: 0.1 eq. triflic acid / CH2Cl2; cyclohexane / 10 - 20 °C
View Scheme
参考文献
Pons; Kocienski
Tetrahedron Letters, 1989 , vol. 30, # 14 p. 1833 - 1836
反应条件
calcium sulfate; silver(l) oxide in benzene
6 h; Ambient temperature;
参考文献
Diolez, Christian; Sarfati, S. Robert; Szabo, Ladislas
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 57 - 60
反应条件
potassium hydroxide in methanol
T=80°C; 2.5 h;
参考文献
Diolez, Christian; Sarfati, S. Robert; Szabo, Ladislas
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 57 - 60
