3-甲氧基苯并[c]色烯-6-酮合成路线 （共 24 条）
反应条件
1: bis-triphenylphosphine-palladium(II) chloride; sodium carbonate / tetrahydrofuran; water / 20 - 80 °C / |Schlenk technique; |Inert atmosphere
2: sodium hydroxide; water / tetrahydrofuran / 80 °C
3: copper (II) acetate monohydrate; tertiary butyl peroxybenzenoate / 1,2-dichloro-ethane / 12 h / 20 - 85 °C
View Scheme
参考文献
Wang, Yang; Gulevich, Anton V.; Gevorgyan, Vladimir
Chemistry - A European Journal, 2013 , vol. 19, # 47 p. 15836 - 15840
反应条件
sulfuric acid; copper; sodium nitrite
ueber das Diazoniumsalz; Behandeln mit Kaliumpermanganat in Aceton;
参考文献
Cavill et al.
Journal of the Chemical Society, 1958 , p. 1544,1548
反应条件
1: diluted NaOH-solution; copper sulfate
2: alkali
View Scheme
参考文献
Hurtley
Journal of the Chemical Society, 1929 , p. 1872
反应条件
boron tribromide in dichloromethane
T=0°C; Inert atmosphere;
参考文献
Nealmongkol, Prattya; Tangdenpaisal, Kassrin; Sitthimonchai, Somkid; Ruchirawat, Somsak; Thasana, Nopporn
Tetrahedron, 2013 , vol. 69, # 44 p. 9277 - 9283
