2,1,3-苯并二唑-4-磺酰氯合成路线 （共 2 条）
反应条件
chlorosulfonic acid T=120 - 130°C; 6 h;
参考文献
Dorogov, Mikhail V.; Filimonov, Sergey I.; Kobylinsky, Dmitry B.; Ivanovsky, Sergey A.; Korikov, Pavel V.; Soloviev, Mikhail Y.; Khahina, Maria Y.; Shalygina, Elena E.; Kravchenko, Dmitry V.; Ivachtchenko, Alexandre V.
Synthesis, 2004 , # 18 p. 2999 - 3004
反应条件
1.1: aq. Na2SO3; NaHCO3 / 0.5 h / 90 °C / pH 9 - 10
1.2: aq. AcOH / 20 °C
2.1: H2O / 20 °C
View Scheme
参考文献
Dorogov, Mikhail V.; Filimonov, Sergey I.; Kobylinsky, Dmitry B.; Ivanovsky, Sergey A.; Korikov, Pavel V.; Soloviev, Mikhail Y.; Khahina, Maria Y.; Shalygina, Elena E.; Kravchenko, Dmitry V.; Ivachtchenko, Alexandre V.
Synthesis, 2004 , # 18 p. 2999 - 3004
