1-[(1S)-3-氯-1-苯基丙氧基]-2-甲基苯合成路线 （共 5 条）
反应条件
triphenylphosphine; diethylazodicarboxylate in tetrahydrofuran Ambient temperature;
参考文献
Srebnik, Morris; Ramachandran, P.V.; Brown, Herbert C.
Journal of Organic Chemistry, 1988 , vol. 53, # 13 p. 2916 - 2920
反应条件
triphenylphosphine; diethylazodicarboxylate in tetrahydrofuran T=20°C; Etherification; Mitsunobu reaction;
参考文献
Liu, Hui-Ling; Hoff, Bard Helge; Anthonsen, Thorleif
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 11 p. 1767 - 1769
反应条件
1: 88 percent / NaBH4 / ethanol / 2 h / 20 °C 2: 51 percent / PPh3; diethyl azodicarboxylate / tetrahydrofuran / 20 °C View Scheme
参考文献
Schneider; Goergens
Tetrahedron Asymmetry, 1992 , vol. 3, # 4 p. 525 - 528
反应条件
1: pH 7, Pseudomonas sp. lipase (SAM-2) 2: Ph3P, DEAD / diethyl ether View Scheme
参考文献
Schneider; Goergens
Tetrahedron Asymmetry, 1992 , vol. 3, # 4 p. 525 - 528
反应条件
1: pyridine / CH2Cl2 2: buffer pH 7 / lipase from Pseudomonas fluorescens (SAM-2) 3: Ph3P, diethylazodicarboxylate View Scheme
参考文献
Schneider; Goergens
Tetrahedron Asymmetry, 1992 , vol. 3, # 4 p. 525 - 528
