反应条件
1: 93 percent / m-chloroperbenzoic acid / CH2Cl2 / 1 h / -78 °C
2: 90 percent / trimethyl phosphite / methanol / 24 h / 22 °C
3: 1.) NaH, 2.) acetyl bromide / 1.) THF, 45 min, 2.) -5 deg C, 3 d
View Scheme
参考文献
Macaulay; Fallis
Journal of the American Chemical Society, 1990 , vol. 112, # 3 p. 1136 - 1144
