反应条件
Multi-step reaction with 4 steps 1: 2.) H2O / 1.) THF, ether, 10 min; 2.) THF, ether, 12 h2: 1.) 1 M LiEt3BH; 2.) 3 M NaOH, 30 percent H2O2 / 1.) THF, 0 deg C, 30 h; 2.) 30 h, RT, water3: 28 percent / PBr3 / diethyl ether / 12 h / 40 °C4: 100 percent / diethyl ether / 0.17 h
参考文献
Dowd, Paul; Hershline, Roger Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1988 , p. 61 - 70
