1: 7.5 g / triethylamine / CH2Cl2 / 1 h / 0 °C 2: 62 percent / tetra-n-butylammonium fluoride / tetrahydrofuran / 1 h / Heating 3: 60 percent / acetic acid / H2O / 1.5 h / Heating View Scheme
参考文献
Rosen, Terry; Chu, Daniel T. W.; Lico, Isabella M.; Fernandes, Prabhavathi B.; Marsh, Kennan; et al.
Journal of Medicinal Chemistry, 1988 , vol. 31, # 8 p. 1598 - 1611
Multi-step reaction with 2 steps 1: 7.5 g / triethylamine / CH2Cl2 / 1 h / 0 °C2: 62 percent / tetra-n-butylammonium fluoride / tetrahydrofuran / 1 h / Heating
参考文献
Rosen, Terry; Chu, Daniel T. W.; Lico, Isabella M.; Fernandes, Prabhavathi B.; Marsh, Kennan; et al. Journal of Medicinal Chemistry, 1988 , vol. 31, # 8 p. 1598 - 1611
Rosen, Terry; Chu, Daniel T. W.; Lico, Isabella M.; Fernandes, Prabhavathi B.; Marsh, Kennan; et al. Journal of Medicinal Chemistry, 1988 , vol. 31, # 8 p. 1598 - 1611
