1147550-11-5合成路线 (共 743 条)
反应条件
1: ammonium thiocyanate With APDPP; bromine in acetonitrile T=20°C; 2 h; 2: 2-(diphenylmethyloxy)tetrahydro-2H-pyran in acetonitrile T=20°C; 24 h;
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 184, # 8 p. 2010 - 2019
反应条件
1: ammonium thiocyanate With PPh3.Br2 in acetonitrile T=20°C; 2: 2-(diphenylmethyloxy)tetrahydro-2H-pyran in acetonitrile T=20°C;
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 180, # 9 p. 2093 - 2096
反应条件
1: ammonium thiocyanate; benzoyl chloride in acetone 0.25 h; Heating; 2: 2-aminopyridine in acetone 0.5 h; Heating;
参考文献
European Journal of Medicinal Chemistry, , vol. 38, # 3 p. 313 - 318
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 181, # 6 p. 1381 - 1389
反应条件
poly[4-diacetoxyiodo]styrene in acetonitrile T=20°C; 1.5 h; regioselective reaction;
参考文献
Wu, Liqiang; Chao, Shujun; Wang, Xiao; Yan, Fulin
Phosphorus, Sulfur and Silicon and the Related Elements, 2011 , vol. 186, # 2 p. 304 - 310
反应条件
PEG-400 in ethyl acetate T=20°C;
参考文献
Wei, Tai-Bao; Li, Man-Lin; Lin, Qi; Liu, Hong; Zhang, You-Ming
Phosphorus, Sulfur and Silicon and the Related Elements, 2006 , vol. 181, # 7 p. 1583 - 1592
反应条件
benzoyl chloride in acetone 0.5 h; Heating;
参考文献
THE BOARD OF TRUSTEES OF THE LELAND STANFORD JUNIOR UNIVERSITY; AUCKLAND UNISERVICES LIMITED
Patent: WO2009/114552 A1, 2009 ;
Location in patent: Page/Page column 86-87 ;
反应条件
ethanol 0.0125 h; Microwave irradiationNeat (no solvent);
参考文献
Uberhande; Thakare; Berad
Journal of the Indian Chemical Society, 2010 , vol. 87, # 9 p. 1137 - 1141
反应条件
und folgendes Erhitzen mit 1 Mol Bleicarbonat auf 120grad in geschlossenen Gefaessen;
参考文献
Gockel
Angewandte Chemie, 1935 , vol. 48, p. 430
Full Text Show Details
Gockel
Patent: DE611945 , 1933 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 21, p. 216
反应条件
hydrogenchloride in water T=100°C; 16 h;
参考文献
THE BOARD OF TRUSTEES OF THE LELAND STANFORD JUNIOR UNIVERSITY; AUCKLAND UNISERVICES LIMITED
Patent: WO2009/114552 A1, 2009 ;
Location in patent: Page/Page column 150-151 ;
反应条件
in acetone 1 h; Heating;
参考文献
Sambaiah, T.; Reddy, K. Kondal
Synthetic Communications, 1990 , vol. 20, # 5 p. 693 - 701