1147550-11-5合成路线 （共 743 条）
参考文献
I.G.Farbenind.
Patent: DE537105 , 1929 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 17, p. 614
参考文献
Werner; Bell
Journal of the Chemical Society, 1920 , vol. 117, p. 1134
Full Text Show Details
Davis; Underwood
Journal of the American Chemical Society, 1922 , vol. 44, p. 2601
反应条件
in water T=80 - 90°C;
参考文献
Vukovic, Nenad; Sukdolak, Slobodan; Solujic, Slavica; Milosevic, Tanja
Archiv der Pharmazie, 2008 , vol. 341, # 8 p. 491 - 496
反应条件
ethanol 0.0125 h; Microwave irradiationNeat (no solvent);
参考文献
Uberhande; Thakare; Berad
Journal of the Indian Chemical Society, 2010 , vol. 87, # 9 p. 1137 - 1141
参考文献
Kurzer; Sanderson
Journal of the Chemical Society, 1957 , p. 4461,4467
反应条件
tetrachloromethane in acetonitrile 10 h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Slagle, J. D.; Huang, T. T.-S.; Franzus, B.
Journal of Organic Chemistry, 1981 , vol. 46, # 17 p. 3526 - 3530
反应条件
bromine; triphenylphosphine in acetonitrile T=20°C; Thiocyanation;
参考文献
Journal of Chemical Research - Part S, , # 11 p. 676 - 677
反应条件
1: ammonium thiocyanate With PPh3.Br2 in acetonitrile T=20°C; 2: 2-tetrahydropyranyl ether of 2-octanol in acetonitrile T=20°C; Title compound not separated from byproducts;
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 180, # 9 p. 2093 - 2096
反应条件
1: ammonium thiocyanate With APDPP; bromine in acetonitrile T=20°C; 2 h; 2: trimethyl(1-methylheptyloxy)silane in acetonitrile T=20°C; 0.0833333 h;
参考文献
Iranpoor, Nasser; Firouzabadi, Habib; Gholinejad, Mohammad
Phosphorus, Sulfur and Silicon and the Related Elements, 2009 , vol. 184, # 8 p. 2010 - 2019
反应条件
1: ammonium thiocyanate With APDPP; bromine in acetonitrile T=20°C; 2 h; 2: 1-methylheptanol; trimethyl(1-methylheptyloxy)silane in acetonitrile T=20°C; 0.0833333 h;
参考文献
Iranpoor, Nasser; Firouzabadi, Habib; Gholinejad, Mohammad
Phosphorus, Sulfur and Silicon and the Related Elements, 2009 , vol. 184, # 8 p. 2010 - 2019
