1147550-11-5合成路线 （共 743 条）
参考文献
Swan
Australian Journal of Scientific Research, Series A: Physical Sciences, 1952 , vol. 5, p. 728,732
反应条件
hydrogenchloride in water T=100°C; 16 h;
参考文献
THE BOARD OF TRUSTEES OF THE LELAND STANFORD JUNIOR UNIVERSITY; AUCKLAND UNISERVICES LIMITED
Patent: WO2009/114552 A1, 2009 ;
Location in patent: Page/Page column 107-108 ;
反应条件
1: 2-bromoaniline hydrochloride With hydrogenchloride in water 0.5 h; Reflux; 2: ammonium thiocyanate in water T=20°C; 4 h; Reflux;
参考文献
Sharma, Pratibha; Kumar, Ashok; Kumari, Prerna; Singh, Jitendra; Kaushik
Medicinal Chemistry Research, 2012 , vol. 21, # 7 p. 1136 - 1148
参考文献
Jackson,F.H.; Peters,A.T.
Journal of the Chemical Society [Section] C: Organic, 1969 , p. 268 - 272
反应条件
hydrogenchloride in water T=100°C; 16 h;
参考文献
THE BOARD OF TRUSTEES OF THE LELAND STANFORD JUNIOR UNIVERSITY; AUCKLAND UNISERVICES LIMITED
Patent: WO2009/114552 A1, 2009 ;
Location in patent: Page/Page column 148 ;
反应条件
hydrogenchloride in water 2 h; Heating;
参考文献
Saxena, Anil K.; Pandey, Suresh K.; Seth; Singh; Dikshit; Carpy
Bioorganic and Medicinal Chemistry, 2001 , vol. 9, # 8 p. 2025 - 2034
反应条件
pyridinium tribromide in acetonitrile T=0 - 20°C; 2 h; regioselective reaction;
参考文献
Wu, Liqiang; Yang, Xiaojuan
Phosphorus, Sulfur and Silicon and the Related Elements, 2012 , vol. 187, # 6 p. 748 - 753
反应条件
1: ammonium thiocyanate With montmorillonite K10 clay in acetone T=20°C; 0.666667 h; 2: 2-bromo-4'-nitroacetophenone T=20°C; 0.00555556 h; Neat (no solvent)Grinding;
参考文献
Meshram; Thakur, Pramod B.; Madhu Babu; Bangade, Vikas M.
Tetrahedron Letters, 2012 , vol. 53, # 14 p. 1780 - 1785
反应条件
bromine in methanol T=5 - 15°C; Industry scale;
参考文献
LUPIN LIMITED; PAGHDAR, Dinesh, Jayntibhai; KOLEKAR, Mahesh, Ramkumar; DESHPANDE, Tushar, Nandkumar; PATIL, Suryaprakash, Pandurang; CHAVAN, Yuvraj, Atmaram; RAY, Purna, Chandra; SINGH, Girij, Pal
Patent: WO2011/158084 A1, 2011 ;
Location in patent: Page/Page column 11 ;
反应条件
bromine; acetic acid
参考文献
Mel'nikow; Tscherkasowa
Zhurnal Obshchei Khimii, 1944 , vol. 14, p. 113
Chem.Abstr., 1945 , p. 934
