1147550-11-5合成路线 (共 743 条)
反应条件
1: ammonium thiocyanate With montmorillonite K10 clay in acetone T=20°C; 0.666667 h; 2: 1-bromomethyl-4-nitro-benzene T=20°C; 0.0666667 h; Neat (no solvent)Grinding;
参考文献
Meshram; Thakur, Pramod B.; Madhu Babu; Bangade, Vikas M.
Tetrahedron Letters, 2012 , vol. 53, # 14 p. 1780 - 1785
反应条件
1: ammonium thiocyanate With APDPP; bromine in acetonitrile T=20°C; 2 h; 2: (4-nitro-phenyl)-methanol in acetonitrile T=20°C; 5 h;
参考文献
Iranpoor, Nasser; Firouzabadi, Habib; Gholinejad, Mohammad
Phosphorus, Sulfur and Silicon and the Related Elements, 2009 , vol. 184, # 8 p. 2010 - 2019
反应条件
1: ammonium thiocyanate With PPh3.Br2 in acetonitrile T=20°C; 2: 4-nitrobenzyl alcohol THP ether in acetonitrile T=20°C;
参考文献
Iranpoor, Nasser; Firouzabadi, Habib; Shaterian, Hamid Reza
Phosphorus, Sulfur and Silicon and the Related Elements, 2005 , vol. 180, # 9 p. 2093 - 2096
反应条件
hydrogenchloride in water T=100°C; 16 h;
参考文献
Li, Liwen; Zhang, Qiu; Liu, Aifeng; Li, Xiue; Zhou, Hongyu; Liu, Yin; Yan, Bing
Journal of the American Chemical Society, 2011 , vol. 133, # 18 p. 6886 - 6889
反应条件
in water 3 h; Heating / reflux; Product distribution / selectivity;
参考文献
YALE UNIVERSITY
Patent: WO2007/38387 A2, 2007 ;
Location in patent: Page/Page column 45; 46 ;
参考文献
Du Pont de Nemours and Co.
Patent: US2883422 , 1958 ;
反应条件
1: With bromine in acetic acid T=0°C; 1.66667 h; 2: With ammonia in water; acetic acid pH=4;
参考文献
Pharmacia and Upjohn Company LLC
Patent: EP1042295 B1, 2005 ;
Location in patent: Page/Page column 131 ;
参考文献
Veszpremi, Tamas; Barta, Istvan; Nagy, Jozsef
Acta Chimica Hungarica, 1986 , vol. 122, # 3-4 p. 243 - 250
反应条件
hydrogenchloride in water
参考文献
Yar, Mohammad Shahar; Ansari, Zaheen Hasan
Acta Poloniae Pharmaceutica - Drug Research, 2009 , vol. 66, # 4 p. 387 - 392
参考文献
Partridge; Short
Journal of the Chemical Society, 1947 , p. 390,391
Full Text Show Details
Oxley; Partridge; Short
Journal of the Chemical Society, 1948 , p. 303,308