1147550-11-5合成路线 （共 743 条）
反应条件
pyridinium tribromide in acetonitrile T=0 - 20°C; 1.5 h; regioselective reaction;
参考文献
Wu, Liqiang; Yang, Xiaojuan
Phosphorus, Sulfur and Silicon and the Related Elements, 2012 , vol. 187, # 6 p. 748 - 753
反应条件
ammonium cerium(IV) nitrate; oxygen in methanol T=0°C; Addition; 0.5 h;
参考文献
Nair, Vijay; Nair, Latha G; George, Tesmol G; Augustine, Anu
Tetrahedron, 2000 , vol. 56, # 38 p. 7607 - 7611
反应条件
in dichloromethane T=20°C;
参考文献
Bhalerao, Dinesh S.; Akamanchi, Krishnacharya G.
Synthetic Communications, 2010 , vol. 40, # 6 p. 799 - 807
反应条件
1: ammonium thiocyanate With benzoyl chloride in acetone HeatingReflux; 2: 3-bromo-aniline in acetone HeatingRefluxCooling with ice; 3: With hydrogenchloride; ammonia; sodium hydroxide in water T=80°C; pH=10; Cooling with ice;
参考文献
THE BOARD OF TRUSTEES OF THE LELAND STANFORD JUNIOR UNIVERSITY; AUCKLAND UNISERVICES LIMITED
Patent: WO2009/114552 A1, 2009 ;
Location in patent: Page/Page column 144 ;
反应条件
1: 3-bromoaniline hydrochloride With hydrogenchloride in water 0.5 h; Reflux; 2: ammonium thiocyanate in water T=20°C; 4 h; Reflux;
参考文献
Sharma, Pratibha; Kumar, Ashok; Kumari, Prerna; Singh, Jitendra; Kaushik
Medicinal Chemistry Research, 2012 , vol. 21, # 7 p. 1136 - 1148
参考文献
Mahapatra
Journal of the Indian Chemical Society, 1956 , vol. 33, p. 923
反应条件
Cu(BF4)2 in water; acetone T=-10 - -5°C;
参考文献
Gorbovoi; Baranovskii; Koval'skii; Grishchuk
Russian Journal of General Chemistry, 2002 , vol. 72, # 8 p. 1230 - 1232
反应条件
bromo-dimethylsulfonium bromide in acetonitrile T=20°C; 0.416667 h;
参考文献
Synlett, , # 19 p. 2952 - 2956
反应条件
1: ammonium thiocyanate With bromine; acetic acid T=10°C; 0.5 h; 2: 4-ethyl-aniline With acetic acid T=10°C; 19 h;
参考文献
European Journal of Organic Chemistry, , # 31 p. 6206 - 6217
反应条件
bromine; acetic acid T=0 - 20°C;
参考文献
Patel, Navin B.; Agravat, Suresh N.; Shaikh, Faiyazalam M.
Medicinal Chemistry Research, 2011 , vol. 20, # 7 p. 1033 - 1041
