1147550-11-5合成路线 （共 743 条）
反应条件
bromine; triphenylphosphine in acetonitrile
T=20°C; Thiocyanation;
参考文献
Iranpoor; Firouzabadi; Shaterian
Journal of Chemical Research - Part S, 1999 , # 11 p. 676 - 677
反应条件
1: ammonium thiocyanate With PPh3.Br2 in acetonitrile
T=20°C;
2: 2-tetrahydropyranyl ether of 2-octanol in acetonitrile
T=20°C; Title compound not separated from byproducts;
参考文献
Iranpoor, Nasser; Firouzabadi, Habib; Shaterian, Hamid Reza
Phosphorus, Sulfur and Silicon and the Related Elements, 2005 , vol. 180, # 9 p. 2093 - 2096
反应条件
1: ammonium thiocyanate With APDPP; bromine in acetonitrile
T=20°C; 2 h;
2: trimethyl(1-methylheptyloxy)silane in acetonitrile
T=20°C; 0.0833333 h;
参考文献
Iranpoor, Nasser; Firouzabadi, Habib; Gholinejad, Mohammad
Phosphorus, Sulfur and Silicon and the Related Elements, 2009 , vol. 184, # 8 p. 2010 - 2019
反应条件
1: ammonium thiocyanate With APDPP; bromine in acetonitrile
T=20°C; 2 h;
2: 1-methylheptanol; trimethyl(1-methylheptyloxy)silane in acetonitrile
T=20°C; 0.0833333 h;
参考文献
Iranpoor, Nasser; Firouzabadi, Habib; Gholinejad, Mohammad
Phosphorus, Sulfur and Silicon and the Related Elements, 2009 , vol. 184, # 8 p. 2010 - 2019
反应条件
T=170 - 175°C; Dimerization; 3 h;
参考文献
Voronkov, M. G.; Vlasova, N. N.; Pestunovich, A. E.
Russian Journal of General Chemistry, 1998 , vol. 68, # 5 p. 770 - 774
Zhurnal Obshchei Khimii, 1998 , vol. 68, # 5 p. 817 - 821
反应条件
1.) acetone, heated water-bath, 1 h, 2.) reflux, 3 h; Yield given. Multistep reaction;
参考文献
Sridevi, G.; Rao, P. Jayaprasad; Reddy, K. Kondal
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1988 , vol. 27, # 1-12 p. 997 - 1000
反应条件
1: ammonium thiocyanate; 1,4-diamino-benzene Neat (no solvent);
2: benzoyl chloride Neat (no solvent);
参考文献
Pourshamsian, Khalil; Montazeri, Naser; Khameneh, Aylar Shams
Asian Journal of Chemistry, 2012 , vol. 24, # 2 p. 837 - 839
参考文献
Budesinsky et al.
Cesko-Slovenska Farmacie, 1959 , vol. 8, p. 129,132
Chem.Abstr., 1960 , p. 3197
反应条件
12-molybdophosphoric acid HPMo; copper dichloride in 1,2-dichloro-ethane
T=20°C; 0.75 h;
参考文献
Chaskar, Atul C.; Yadav, Arun A.; Langi, Bhushan P.; Murugappan, Anita; Shah, Chetan
Synthetic Communications, 2010 , vol. 40, # 19 p. 2850 - 2856
反应条件
in water
T=80 - 90°C;
参考文献
Vukovic, Nenad; Sukdolak, Slobodan; Solujic, Slavica; Milosevic, Tanja
Archiv der Pharmazie, 2008 , vol. 341, # 8 p. 491 - 496
