1147550-11-5合成路线 （共 743 条）
反应条件
T=170 - 175°C; Dimerization; 3 h;
参考文献
Voronkov, M. G.; Vlasova, N. N.; Pestunovich, A. E.
Russian Journal of General Chemistry, 1998 , vol. 68, # 5 p. 770 - 774
Zhurnal Obshchei Khimii, 1998 , vol. 68, # 5 p. 817 - 821
参考文献
Young
Chemische Berichte, 1892 , vol. 25, p. 2106
反应条件
in acetone
T=15 - 35°C; 4 h;
参考文献
AB SCIENCE
Patent: WO2008/98949 A2, 2008 ;
Location in patent: Page/Page column 18; 19 ;
WO 2008/098949 A2
反应条件
1: 2-methyl-5-chloroaniline With hydrogenchloride in water
0.5 h; Reflux;
2: ammonium thiocyanate in water
4 h; Reflux;
参考文献
Sharma, Praveen Kumar; Fogla, Ankur; Rathore; Kumar
Research on Chemical Intermediates, 2011 , vol. 37, # 8 p. 1103 - 1111
参考文献
Hoffmann-La Roche
Patent: DE377412 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 14, p. 1378
反应条件
in 3-methyl-1-butanol
2 h; Heating;
参考文献
Purushothaman; Rajasekharan Pillai
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1990 , vol. 29, # 1 p. 18 - 21
反应条件
bromine in acetic acid
0.25 h;
参考文献
Mangold; Hanna
Journal of Medicinal Chemistry, 1982 , vol. 25, # 6 p. 630 - 638
参考文献
v.Braun; Lemke
Chemische Berichte, 1922 , vol. 55, p. 3553
参考文献
Wu; Waksmunski; Hoff; Fisher; Egerton; Patchett
Journal of Pharmaceutical Sciences, 1977 , vol. 66, # 8 p. 1150 - 1153
参考文献
Behaghel; Schneider
Chemische Berichte, 1936 , vol. 69, p. 88,92
