1147550-11-5合成路线 (共 743 条)
反应条件
1: furan-2-carbonyl chloride; ammonium thiocyanate in acetone
T=30°C; 0.166667 h;
2: diethylamine in acetone
10 h; Heating; Further stages.;
参考文献
Otazo-Sanchez, Elena; Perez-Marin, Leonel; Estevez-Hernandez, Osvaldo; Rojas-Lima, Susana; Alonso-Chamarro, Julian
Journal of the Chemical Society. Perkin Transactions 2, 2001 , # 11 p. 2211 - 2218
反应条件
1: furan-2-carbonyl chloride; ammonium thiocyanate in acetone
T=30°C; 0.166667 h;
2: p-toluidine in acetone
0.166667 h; Heating; Further stages.;
参考文献
Otazo-Sanchez, Elena; Perez-Marin, Leonel; Estevez-Hernandez, Osvaldo; Rojas-Lima, Susana; Alonso-Chamarro, Julian
Journal of the Chemical Society. Perkin Transactions 2, 2001 , # 11 p. 2211 - 2218
反应条件
in hydrogenchloride
T=80°C; 1.5 h;
参考文献
Richter; Oertel
Pharmazie, 1990 , vol. 45, # 10 p. 721 - 724
反应条件
PEG-400 in ethyl acetate
T=20°C;
参考文献
Wei, Tai-Bao; Li, Man-Lin; Lin, Qi; Liu, Hong; Zhang, You-Ming
Phosphorus, Sulfur and Silicon and the Related Elements, 2006 , vol. 181, # 7 p. 1583 - 1592
反应条件
PEG-400 in ethyl acetate
T=20°C;
参考文献
Wei, Tai-Bao; Li, Man-Lin; Lin, Qi; Liu, Hong; Zhang, You-Ming
Phosphorus, Sulfur and Silicon and the Related Elements, 2006 , vol. 181, # 7 p. 1583 - 1592
反应条件
PEG-400 in dichloromethane
T=20°C; Substitution; 1 h;
参考文献
Lin, Qi; Yao, Hong; Wei, Tai-Bao; Zhang, You-Ming
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2009 , vol. 48, # 1 p. 124 - 127
反应条件
tetrabutylammomium bromide in acetone
0.75 h; Reflux;
参考文献
Saeed, Sohail; Hussain, Rizwan; Ali, Muhammad
Journal of Heterocyclic Chemistry, 2013 , vol. 50, # 2 p. 237 - 243
反应条件
1: ammonium thiocyanate; 4-methoxy-benzoyl chloride With PEG-400 in dichloromethane
2: 1-Bromo-2-aminobenzene in dichloromethane
Further stages.;
参考文献
Wang, Junke; Peng, Feng; Jiang, Ju-li; Lu, Zhi-jin; Wang, Le-yong; Bai, Junfeng; Pan, Yi
Tetrahedron Letters, 2008 , vol. 49, # 3 p. 467 - 470
反应条件
1: ammonium thiocyanate; 4-methyl-benzoyl chloride in acetone
T=30°C; 0.166667 h;
2: aniline in acetone
0.166667 h; Heating; Further stages.;
参考文献
Otazo-Sanchez, Elena; Perez-Marin, Leonel; Estevez-Hernandez, Osvaldo; Rojas-Lima, Susana; Alonso-Chamarro, Julian
Journal of the Chemical Society. Perkin Transactions 2, 2001 , # 11 p. 2211 - 2218
反应条件
1: ammonium thiocyanate With bromine; acetic acid
T=10°C; 0.5 h;
2: 1-amino-2,4-dimethoxy-benzene With acetic acid
T=10°C; 19 h;
参考文献
Hirose, Wataru; Sato, Kousuke; Matsuda, Akira
European Journal of Organic Chemistry, 2011 , # 31 p. 6206 - 6217