1147550-11-5合成路线 (共 743 条)
反应条件
copper diacetate in water; acetone
Substitution; Product distribution; Further Variations:effect of absence of Cu salt;
参考文献
Grishchuk; Gorbovoi; Zagrichuk; Ganushchak; Kudrik
Russian Journal of General Chemistry, 1999 , vol. 69, # 8 p. 1299 - 1303
反应条件
aluminum oxide; methanesulfonic acid
T=20°C; 0.166667 h; neat (no solvent); regioselective reaction;
参考文献
Hosseini-Sarvari, Mona; Tavakolian, Mina
Journal of Chemical Research, 2008 , # 6 p. 318 - 321
反应条件
1: ammonium thiocyanate; benzoyl chloride in acetone
0.25 h; Heating;
2: 1-Bromo-2-aminobenzene in acetone
0.5 h; Heating;
参考文献
Wang, Junke; Peng, Feng; Jiang, Ju-li; Lu, Zhi-jin; Wang, Le-yong; Bai, Junfeng; Pan, Yi
Tetrahedron Letters, 2008 , vol. 49, # 3 p. 467 - 470
反应条件
1: ammonium thiocyanate; benzoyl chloride With PEG-400 in dichloromethane
T=20°C; 1 h;
2: 4-amino-phenol in dichloromethane
2 h;
参考文献
Zhang; Wei; Gao
Synthetic Communications, 2001 , vol. 31, # 20 p. 3099 - 3105
反应条件
1: furan-2-carbonyl chloride; ammonium thiocyanate in acetone
T=30°C; 0.166667 h;
2: 4-ethoxy-aniline in acetone
0.166667 h; Heating; Further stages.;
参考文献
Otazo-Sanchez, Elena; Perez-Marin, Leonel; Estevez-Hernandez, Osvaldo; Rojas-Lima, Susana; Alonso-Chamarro, Julian
Journal of the Chemical Society. Perkin Transactions 2, 2001 , # 11 p. 2211 - 2218
参考文献
Saeed, Aamer; Floerke, Ulrich; Erben, Mauricio F.
Journal of Molecular Structure, 2014 , vol. 1065-1066, # 1 p. 150 - 159
反应条件
1.) Me2CO, 40 deg C, 30 min, 2.) Me2CO, 20 deg C, 2 h; Yield given. Multistep reaction;
参考文献
Brindley, Jocelyn C.; Caldwell, Jennifer M.; Meakins, G. Denis; Plackett, Simon J.; Price, Susan J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 1153 - 1158
反应条件
tetra(n-butyl)ammonium hydrogensulfate in dichloromethane; water
14 h;
参考文献
Weitzberg, Moshe; Aizenshtat, Zeev; Blum, Jochanan
Journal of Heterocyclic Chemistry, 1984 , vol. 21, p. 1597 - 1601
反应条件
1: ammonium thiocyanate With montmorillonite K10 clay in acetone
T=20°C; 0.666667 h;
2: 2-bromo-1-(3',4-dichlorophenyl)acetophenone T=20°C; 0.00555556 h; Neat (no solvent)Grinding;
参考文献
Meshram; Thakur, Pramod B.; Madhu Babu; Bangade, Vikas M.
Tetrahedron Letters, 2012 , vol. 53, # 14 p. 1780 - 1785
反应条件
1: ammonium thiocyanate; meta-chlorobenzoyl chloride in acetone
T=30°C; 0.166667 h;
2: aniline in acetone
0.166667 h; Heating; Further stages.;
参考文献
Otazo-Sanchez, Elena; Perez-Marin, Leonel; Estevez-Hernandez, Osvaldo; Rojas-Lima, Susana; Alonso-Chamarro, Julian
Journal of the Chemical Society. Perkin Transactions 2, 2001 , # 11 p. 2211 - 2218