1147550-11-5合成路线 （共 743 条）
反应条件
1: ammonium thiocyanate; 4-nitro-benzoyl chloride in acetone
T=30°C; 0.166667 h;
2: aniline in acetone
0.166667 h; Heating; Further stages.;
参考文献
Otazo-Sanchez, Elena; Perez-Marin, Leonel; Estevez-Hernandez, Osvaldo; Rojas-Lima, Susana; Alonso-Chamarro, Julian
Journal of the Chemical Society. Perkin Transactions 2, 2001 , # 11 p. 2211 - 2218
反应条件
1. acetone, 5 min, reflux; Yield given. Multistep reaction;
参考文献
Kavalek, Jaromir; Jirman, Josef; Machacek, Vladimir; Sterba, Vojeslav
Collection of Czechoslovak Chemical Communications, 1988 , vol. 53, # 3 p. 593 - 600
反应条件
bromine; triphenylphosphine in acetonitrile
T=20°C; Thiocyanation;
参考文献
Azadi, Roya; Mokhtari, Babak; Makaremi, Mohamad-Ali
Chinese Chemical Letters, 2012 , vol. 23, # 1 p. 77 - 80
反应条件
1: ammonium thiocyanate With bromine; triphenylphosphine in acetonitrile
T=20°C; Addition;
2: PhCH2CH2OTMS in acetonitrile
T=20°C; Substitution;
参考文献
Iranpoor; Firouzabadi; Shaterian
Synlett, 2000 , # 1 p. 65 - 66
反应条件
1: ammonium thiocyanate With bromine; triphenylphosphine in acetonitrile
T=20°C; Addition;
2: butyl-dimethyl-phenethyloxy-silane in acetonitrile
T=20°C; Substitution;
参考文献
Iranpoor; Firouzabadi; Shaterian
Synlett, 2000 , # 1 p. 65 - 66
反应条件
1: ammonium thiocyanate With PPh3.Br2 in acetonitrile
T=20°C;
2: tetrahydro-2-(2-phenylethoxy)-2H-pyran in acetonitrile
T=20°C;
参考文献
Iranpoor, Nasser; Firouzabadi, Habib; Shaterian, Hamid Reza
Phosphorus, Sulfur and Silicon and the Related Elements, 2005 , vol. 180, # 9 p. 2093 - 2096
反应条件
hydrogenchloride; acetic acid
aufeinanderfolgend Umsetzung;
参考文献
Jackman et al.
Journal of the American Chemical Society, 1948 , vol. 70, p. 2884
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Haurowitz et al.
Journal of Biological Chemistry, 1957 , vol. 224, p. 827,828,829
反应条件
N-bromosuccinmide in acetonitrile
T=20°C; 5 h;
参考文献
Reddy, B.V. Subba; Reddy, S. Madhu Sudana; Madan, Ch.
Tetrahedron Letters, 2011 , vol. 52, # 13 p. 1432 - 1435
参考文献
Partridge; Short
Journal of the Chemical Society, 1947 , p. 390,391
反应条件
acetic anhydride; acetic acid
T=60 - 100°C; 2 h;
参考文献
Papeo, Gianluca; Posteri, Helena; Borghi, Daniela; Varasi, Mario
Organic Letters, 2005 , vol. 7, # 25 p. 5641 - 5644
