1147550-11-5合成路线 (共 743 条)
反应条件
1: ammonium thiocyanate With montmorillonite K10 clay in acetone T=20°C; 0.666667 h; 2: 2-(Bromoacetyl)furan T=20°C; 0.00833333 h; Neat (no solvent)Grinding;
参考文献
Meshram; Thakur, Pramod B.; Madhu Babu; Bangade, Vikas M.
Tetrahedron Letters, 2012 , vol. 53, # 14 p. 1780 - 1785
参考文献
Sam; Valentine; Richmond
Journal of pharmaceutical sciences, 1968 , vol. 57, # 10 p. 1763 - 1768
反应条件
bromine; triphenylphosphine in acetonitrile T=20°C; Thiocyanation;
参考文献
Iranpoor; Firouzabadi; Shaterian
Journal of Chemical Research - Part S, 1999 , # 11 p. 676 - 677
反应条件
1: ammonium thiocyanate With bromine; triphenylphosphine in acetonitrile T=20°C; Addition; 2: 4-Cl-C6H4CH2OTMS in acetonitrile T=20°C; Substitution;
参考文献
Iranpoor; Firouzabadi; Shaterian
Synlett, 2000 , # 1 p. 65 - 66
反应条件
1: ammonium thiocyanate With PPh3.Br2 in acetonitrile T=20°C; 2: p-(Cl)C6H4CH2OTHP in acetonitrile T=20°C;
参考文献
Iranpoor, Nasser; Firouzabadi, Habib; Shaterian, Hamid Reza
Phosphorus, Sulfur and Silicon and the Related Elements, 2005 , vol. 180, # 9 p. 2093 - 2096
反应条件
1.) Me2CO, 40 deg C, 30 min, 2.) Me2CO, 20 deg C, 2 h; Yield given. Multistep reaction;
参考文献
Brindley, Jocelyn C.; Caldwell, Jennifer M.; Meakins, G. Denis; Plackett, Simon J.; Price, Susan J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 1153 - 1158
反应条件
1: ammonium thiocyanate; benzoyl chloride With tetrabutylammomium bromide in acetone Reflux; 2: 4-bromo-aniline in acetone 1.5 h; Reflux;
参考文献
Saeed, Sohail; Rashid, Naghmana; Bhatti, Moazzam Hussain; Jones, Peter G.
Turkish Journal of Chemistry, 2010 , vol. 34, # 5 p. 761 - 770
反应条件
hydrogenchloride in water 1.) 25 deg C, 0.5 h, 2.) reflux, 3 h;
参考文献
Nasipuri, Dhanonjoy; Banerjee, Satinath; Alaka, B. V.; Daw, N. P.
Synthesis, 1982 , # 12 p. 1073 - 1075
反应条件
iron(III) chloride in dichloromethane T=20°C; 4 h;
参考文献
Yadav; Reddy; Krishna; Suresh Reddy; Narsaiah
Synthesis, 2005 , # 6 art. no. Z16504SS, p. 961 - 964
反应条件
1: ammonium thiocyanate; benzoyl chloride in acetone 0.25 h; Heating; 2: 3-chloro-aniline in acetone 0.5 h; Heating;
参考文献
Narayana; Ashalatha; Vijaya Raj; Suchetha Kumari
Phosphorus, Sulfur and Silicon and the Related Elements, 2006 , vol. 181, # 6 p. 1381 - 1389