反应条件
1: 1.) dimethyl disulfide, 2.) n-Bu3P / 1.) CH2Cl2, 0 deg C, 4 h, 2.) methanol, water, 25 deg C, 1 h
2: NaH / tetrahydrofuran / Ambient temperature
3: 74 percent / MCPBA / CH2Cl2 / 0.5 h / 0 °C
View Scheme
参考文献
Anderson, M.B.; Ranasinghe, M.G.; Palmer, J.T.; Fuchs, P.L.
Journal of Organic Chemistry, 1988 , vol. 53, # 13 p. 3125 - 3127
