反应条件
Multi-step reaction with 3 steps 1: hydroxylamine hydrochloride; sodium carbonate / ethanol; water / 120 h / 25 °C2: sulfuric acid; N,N,N,N',N',N'-hexamethyl-butane-1,4-diammonium dimethylsulfate / methanol; water / 50 °C / Electrochemical reduction3: triethylamine / dichloromethane / 0 - 20 °C
参考文献
Kulisch, Joern; Nieger, Martin; Stecker, Florian; Fischer, Andreas; Waldvogel, Siegfried R. Angewandte Chemie - International Edition, 2011 , vol. 50, # 24 p. 5564 - 5567