4-甲氧基-3-甲基苄醇合成路线 （共 10 条）
反应条件
1: With sodium tetrahydroborate in ethanol 2: With water in ethanol
参考文献
ELI LILLY AND COMPANY
Patent: WO2005/54176 A1, 2005 ;
Location in patent: Page/Page column 103 ;
WO 2005/054176 A1
反应条件
1: 1.) Mg / 1.) THF, 2.) THF, reflux, 5 min 2: NaBH4 / methanol / 0.25 h / Ambient temperature View Scheme
参考文献
Synthetic Communications, , vol. 22, # 17 p. 2571 - 2578
反应条件
acetic acid Kochen des Reaktionsprodukts mit wss.-aethanol. KOH;
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 204, p. 130
Bulletin de la Societe Chimique de France, , vol. <5> 4, p. 1092,1095
反应条件
triphenylphosphine in dichloromethane
参考文献
Banker, Pierette; Cadilla, Rodolfo; Lambert lll, Millard Hurst; Rafferty, Stephen William; Sternbach, Daniel David; Sznaidman, Marcos Luis
Patent: US2004/72838 A1, 2004 ;
US 20040072838 A1
反应条件
Petroleum ether Einleiten von HCl;
参考文献
Baddeley et al.
Journal of the Chemical Society, 1956 , p. 2455,246
反应条件
1: diethyl ether; aqueous HCl 2: Erhitzen unter Normaldruck auf Siedetemperatur View Scheme
参考文献
Quelet; Allard
Bulletin de la Societe Chimique de France, 1937 , vol. <5> 4, p. 1468,1470
反应条件
1: diethyl ether; aqueous HCl 2: Erhitzen unter Normaldruck auf Siedetemperatur View Scheme
参考文献
Quelet; Allard
Bulletin de la Societe Chimique de France, 1937 , vol. <5> 4, p. 1468,1470
反应条件
1: PBr3, pyridine / 3 h / Ambient temperature 2: 18-crown-6 / acetonitrile / 9 h / 60 °C View Scheme
参考文献
Burnell; Dumont; Theberge; Desfosses
Synthetic Communications, 1992 , vol. 22, # 17 p. 2571 - 2578
反应条件
permanganate(VII) ion
参考文献
Bulletin de la Societe Chimique de France, , vol. <5> 4, p. 1092,1095
反应条件
pyridine; phosphorus tribromide 3 h; Ambient temperature;
参考文献
Kelley; Linn; Selway
Journal of Medicinal Chemistry, 1989 , vol. 32, # 8 p. 1757 - 1763
