3-(3-氧代丙基)苯甲酸乙酯合成路线 (共 2 条)
反应条件
tetrabutylammomium bromide; palladium diacetate; sodium hydrogencarbonate in N,N-dimethyl-formamide T=70°C; 3 h; Inert atmosphereMolecular sieve;
参考文献
Gesinski, Michael R.; Tadpetch, Kwanruthai; Rychnovsky, Scott D.
Organic Letters, 2009 , vol. 11, # 22 p. 5342 - 5345
反应条件
1: 92 percent / (PH3P)2PdCl2, CuI, Et2NH / 1.5 h / Ambient temperature 2: 91 percent / H2 / 5percent Pd/C / ethanol / 3 h / 760 Torr 3: 55 percent / pyridinium chlorochromate / CH2Cl2 / 4 h / Ambient temperature View Scheme
参考文献
Chuang, Che-Ping; Gallucci, Judith C.; Hart, David J.
Journal of Organic Chemistry, 1988 , vol. 53, # 14 p. 3210 - 3218