烯丙基2-脱氧-2-(1,3-二氧代-1,3-二氢-2H-异吲哚-2-基)-beta-D-苏-吡喃己糖苷合成路线 （共 5 条）
反应条件
hydrogenchloride in acetone T=70°C;
参考文献
Wang, Lai-Xi; Li, Chuan; Wang, Qin-Wei; Hui, Yong-Zheng
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 6 p. 621 - 628
反应条件
1: 96 percent / HBr / acetic acid 2: 74 percent / Hg(CN)2 3: 53 percent / aq. HCl / acetone View Scheme
参考文献
Journal of Carbohydrate Chemistry, , vol. 13, # 5 p. 819 - 824
反应条件
1.1: triethylamine; pyridine / 1.25 h / 20 °C 1.2: 0.17 h / 90 - 95 °C 2.1: tin(IV) chloride / dichloromethane / 55 h / 0 - 20 °C / Inert atmosphere 3.1: acetyl chloride; methanol / 50.08 h / 0 - 20 °C View Scheme
反应条件
1.1: triethylamine; pyridine / 1.25 h / 20 °C 1.2: 0.17 h / 90 - 95 °C 2.1: tin(IV) chloride / dichloromethane / 55 h / 0 - 20 °C / Inert atmosphere 3.1: acetyl chloride; methanol / 50.08 h / 0 - 20 °C View Scheme
反应条件
1: 74 percent / Hg(CN)2 2: 53 percent / aq. HCl / acetone View Scheme
参考文献
Journal of Carbohydrate Chemistry, , vol. 13, # 5 p. 819 - 824
