4-((E)-苯乙烯基)-苯甲酸甲酯合成路线 （共 45 条）
反应条件
1: NaOMe / methanol
2: Irradiation
View Scheme
参考文献
Mulzer, Johann; Boehm, Ingo; Bats, Jan-W
Tetrahedron Letters, 1998 , vol. 39, # 52 p. 9643 - 9646
反应条件
1: NaOMe / methanol
2: Irradiation
View Scheme
参考文献
Mulzer, Johann; Boehm, Ingo; Bats, Jan-W
Tetrahedron Letters, 1998 , vol. 39, # 52 p. 9643 - 9646
反应条件
Kyowaad 2200 hydrocalcite clay
1.) water, RT, irradiation, 8 h, 2.) ethyl ether; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Takagi, Katsuhiko; Shichi, Tetsuya; Usami, Hisanao; Sawaki, Yasuhiko
Journal of the American Chemical Society, 1993 , vol. 115, # 10 p. 4339 - 4344
反应条件
1: 49 percent / kBuOK / dimethylformamide / 0.25 h
2: 1) HCl, 2) H2O / 1) 36 h, room temperature, 2) 2 h, 40 deg C
View Scheme
参考文献
Schiemenz, Guenter Paulus; Finzenhagen, Manfred
Liebigs Annalen der Chemie, 1981 , # 8 p. 1476 - 1484
反应条件
1: 49 percent / kBuOK / dimethylformamide / 0.25 h
2: 1) HCl, 2) H2O / 1) 36 h, room temperature, 2) 2 h, 40 deg C
View Scheme
参考文献
Schiemenz, Guenter Paulus; Finzenhagen, Manfred
Liebigs Annalen der Chemie, 1981 , # 8 p. 1476 - 1484
反应条件
1: caesium carbonate; tris-(dibenzylideneacetone)dipalladium(0); trifuran-2-yl-phosphane / 1,4-dioxane; water / 65 °C / |Inert atmosphere
2: bis-triphenylphosphine-palladium(II) chloride; sodium tetrahydroborate; N,N,N',N,-tetramethylethylenediamine / tetrahydrofuran / 30 h / 25 °C / |Inert atmosphere
View Scheme
参考文献
Chelucci, Giorgio
Chemical Communications, 2014 , vol. 50, # 31 p. 4069 - 4072
反应条件
1.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / 20 °C / Inert atmosphere
2.1: FeH(CO)(NO)(PPh3)2; phenyl silane; triethylamine / tetrahydrofuran / 40 °C
2.2: 2 h / 0 °C / Inert atmosphere
View Scheme
参考文献
Belger, Christian; Plietker, Bernd
Chemical Communications, 2012 , vol. 48, # 44 p. 5419 - 5421
反应条件
1: water; acetone / Versetzen des Reaktionsgemisches mit wss. Kupfer(II)-chlorid-Loesung
2: diethyl ether
View Scheme
参考文献
Kon
Journal of the Chemical Society, 1948 , p. 224,225
反应条件
1: water; acetone / Versetzen des Reaktionsgemisches mit wss. Kupfer(II)-chlorid-Loesung
2: diethyl ether
View Scheme
参考文献
Kon
Journal of the Chemical Society, 1948 , p. 224,225
参考文献
Kon
Journal of the Chemical Society, 1948 , p. 224,225
