2,6-二甲基吡啶-3,5-二甲酸二乙酯合成路线 (共 142 条)
反应条件
hydrogenchloride in dichloromethane 2 h; Ambient temperature; Yield given;
参考文献
Heterocycles, , vol. 37, # 2 p. 815 - 822
反应条件
bentonite K10 clay in ethanol 2 h; Heating; Yield given;
参考文献
Bulletin des Societes Chimiques Belges, , vol. 104, # 6 p. 387 - 392
反应条件
[Pt(II)(substituted terpyridyl)]ClO4 in acetonitrile UV-irradiation; KineticsQuantum yield;
参考文献
Journal of the American Chemical Society, , vol. 126, # 11 p. 3440 - 3441
反应条件
ammonium hydroxide T=140°C; Hantzsch synthesis; 0.166667 h; microwave irradiation; Title compound not separated from byproducts;
参考文献
Synthesis, , # 8 p. 1283 - 1288
反应条件
acetic acid T=100°C;
参考文献
Gazzetta Chimica Italiana, , vol. 89, p. 2151,2161
反应条件
acetic acid Condensation; addition; 1 h; Heating;
参考文献
Chemistry of Heterocyclic Compounds, , vol. 35, # 6 p. 688 - 694
反应条件
in benzene-d6 T=50°C; 8 h; Inert atmosphereSchlenk technique;
参考文献
Angewandte Chemie - International Edition, , vol. 51, # 50 p. 12564 - 12569
Angew. Chem., , vol. 124, # 50 p. 12732 - 12737,6
反应条件
zinc(II) chloride T=100°C; im Rohr;
参考文献
Chemische Berichte, , vol. 21, p. 2740
反应条件
in pyridine 6 h; Heating;
参考文献
Russian Chemical Bulletin, , vol. 44, # 7 p. 1272 - 1275
Izvestiya Akademi Nauk, Seriya Khimicheskaya, , # 7 p. 1318 - 1321
反应条件
in acetonitrile T=20°C; Reduction; oxidation; 17 h; Kinetics; Further Variations:Temperatures;
参考文献
Journal of the Chemical Society. Perkin Transactions 2, , # 9 p. 1857 - 1861