2-甲基-3-丁烯-2-醇合成路线 （共 471 条）
反应条件
boron trifluoride diethyl etherate in 1,4-dioxane T=20°C; 72 h;
参考文献
Helesbeux, Jean-Jacques; Duval, Olivier; Guilet, David; Seraphin, Denis; Rondeau, David; Richomme, Pascal
Tetrahedron, 2003 , vol. 59, # 27 p. 5091 - 5104
反应条件
mesoporous silica containing bimetallic Cu-Al (CuAl-KIT-5) in 1,2-dichloro-ethane T=60°C; 6 h;
参考文献
Varghese, Shaji; Anand, Chokkalingam; Dhawale, Dattatray; Mane, Gurudas P.; Wahab, Mohammad A.; Mano, Ajayan; Raj, George Allen Gnana; Nagarajan, Samuthira; Vinu, Ajayan
ChemCatChem, 2013 , vol. 5, # 4 p. 899 - 902
反应条件
CuAl-SBA-15 in cyclohexane T=85°C; 16 h;
参考文献
Varghese, Shaji; Anand, Chokkalinkam; Dhawale, Dattatray; Mano, Ajayan; Balasubramanian, Veerappan V.; Raj, George Allen Gnana; Nagarajan, Samuthira; Wahab, Mohammad A.; Vinu, Ajayan
Tetrahedron Letters, 2012 , vol. 53, # 42 p. 5656 - 5659
反应条件
potassium hydroxide; air; aluminosilicate ASHNTS-3 1) octane, reflux, 2) H2O-CH3OH; Yield given. Multistep reaction;
参考文献
Byzova, V. N.; Zakharova, E. I.; Zhukova, E. E.; Sarycheva, I. K.; Evstigneeva, R. P.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, # 11 p. 2135 - 2140
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 11 p. 2368 - 2374
反应条件
tributylphosphine in dichloromethane-d2 T=35°C; 18 h;
参考文献
Vedejs, E.; Bennett, N. S.; Conn, L. M.; Diver, S. T.; Gingras, M.; et al.
Journal of Organic Chemistry, 1993 , vol. 58, # 25 p. 7286 - 7288
反应条件
N,N-dimethyl-aniline in diethyl ether
参考文献
Vedejs, E.; Bennett, N. S.; Conn, L. M.; Diver, S. T.; Gingras, M.; et al.
Journal of Organic Chemistry, 1993 , vol. 58, # 25 p. 7286 - 7288
反应条件
hydrogenchloride in methanol Heating;
参考文献
Mukai, Kazuo; Takamatsu, Kimiko; Ishizu, Kazuhiko
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 12 p. 3507 - 3510
反应条件
1: With formic acid in tetrahydrofuran T=100°C; 3 h; 2: With hydrogenchloride in methanol T=60°C; 0.333333 h; Further stages.;
参考文献
Patel, Anjan; Liebner, Falk; Netscher, Thomas; Mereiter, Kurt; Rosenau, Thomas
Journal of Organic Chemistry, 2007 , vol. 72, # 17 p. 6504 - 6512
参考文献
Fairhurst, Shirley A.; Sutcliffe, Leslie H.; Taylor, Sheila M.
Journal of the Chemical Society, Faraday Transactions 1: Physical Chemistry in Condensed Phases, 1982 , vol. 78, p. 2743 - 2756
反应条件
1: chloroform; chlorine / -10 - -5 °C 2: P2O5 / 98 °C / 100 Torr 3: alcoholic KOH; hydroquinone View Scheme
参考文献
Petrow
Zhurnal Obshchei Khimii, 1943 , vol. 13, p. 741,748
Zhurnal Obshchei Khimii, 1945 , vol. 15, p. 931,937
Chem.Abstr., 1945 , p. 696,1946 6415
