2-甲基-3-丁烯-2-醇合成路线 (共 471 条)
反应条件
copper(l) iodide; boron trifluoride diethyl etherate Yield given. Yields of byproduct given;
参考文献
Yamamoto, Yoshinori; Yamamoto, Shinichi; Yatagai, Hidetaka; Maruyama, Kazuhiro
Journal of the American Chemical Society, 1980 , vol. 102, # 7 p. 2318 - 2325
反应条件
hydroxide T=22.85°C; P=740 Torr; Kinetics;
参考文献
Baker, Jillian; Arey, Janet; Atkinson, Roger
Journal of Physical Chemistry A, 2004 , vol. 108, # 34 p. 7032 - 7037
反应条件
phosphoric acid in Petroleum ether T=35 - 40°C; 4 h;
参考文献
Ahluwalia, V. K.; Arora, K. K.; Anand, Saroj
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 2 p. 129 - 131
反应条件
formic acid 4 h; Heating;
参考文献
Wang, Qiaoling; She, Xuegong; Ren, Xinfeng; Ma, Junying; Pan, Xinfu
Tetrahedron Asymmetry, 2004 , vol. 15, # 1 p. 29 - 34
反应条件
cyclic polyphosphate ester in chloroform 7 h; Ambient temperature;
参考文献
Al-Khayat, Isam; Dean, Francis M.; France, Steven N.; Matkin, David A.; Orabi, Mohamed O. A.; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1301 - 1310
反应条件
in diethyl ether adding N-N'-ligand (30percent molar excess) and olefin to soln./suspn. of dimethyl sulfide complex in diethyl ether, stirring (15 h, room temp.), pptn.; filtering, drying, recrystn. (methylene chloride - diethyl ether);
参考文献
Cucciolito, Maria Elena; Felice, Vincenzo De; Panunzi, Achille; Vitagliano, Aldo
Organometallics, 1989 , vol. 8, p. 1180 - 1187
反应条件
hydrogen; ruthenium palladium in propan-1-ol T=89.9°C; Rate constant;
参考文献
Karavanov, A. N.; Gryaznov, V. M.; Batyrev, I. G.; Olenina, E. G.
Russian Journal of Physical Chemistry, 1995 , vol. 69, # 5 p. 739 - 743
Zhurnal Fizicheskoi Khimii, 1995 , vol. 69, # 5 p. 816 - 821
反应条件
palladium diacetate; triphenylphosphine-3,3',3''-trisulfonic acid trisodium salt; triethylamine T=130°C; Heck reaction, debromiation; 8 h;
参考文献
Tetrahedron Letters, , vol. 40, # 44 p. 7803 - 7806
反应条件
cerium (III) nitrate hexahydrate; dihydrogen peroxide; lithium bromide in water T=65 - 70°C; 10 h;
参考文献
Russian Chemical Bulletin, , vol. 61, # 2 p. 459 - 463
Izv. Akad. Nauk, Ser. Khim., , # 2 p. 456 - 460,5
反应条件
in acetonitrile T=-27.1°C; Irradiationother allylic alcohols, other spin-trap compounds: 2,4,6-tribromonitrosobenzene, 3,5-dibromo-4-nitrosobenzenesulfonic acid, other temperature; MechanismProduct distribution;
参考文献
Grossi, Loris; Strazzari, Samantha; Gilbert, Bruce C.; Whitwood, Adrian C.
Journal of Organic Chemistry, 1998 , vol. 63, # 23 p. 8366 - 8372