2-甲基-3-丁烯-2-醇合成路线 （共 471 条）
反应条件
1.1: 4-(N,N-dimethlyamino)pyridine; triethylamine / dichloromethane / 36 h / 20 °C / |Inert atmosphere 2.1: bis(dibenzylideneacetone)-palladium(0) / 0.08 h / |Inert atmosphere; |Sealed tube 2.2: 24 h / 50 °C / |Inert atmosphere; |Sealed tube View Scheme
参考文献
Beveridge, Ramsay E.; Batey, Robert A.
Organic Letters, 2014 , vol. 16, # 9 p. 2322 - 2325
反应条件
toluene-4-sulfonic acid; hydroquinone
参考文献
Cresson,P.
Bulletin de la Societe Chimique de France, 1964 , p. 2618 - 2628
反应条件
di-tert-butyl phosphite; dibenzoyl peroxide in cyclohexane T=80°C;
参考文献
Barks; Gilbert; Parsons; Upeandran
Synlett, 2001 , # 11 p. 1719 - 1722
反应条件
dibenzoyl peroxide Heating;
参考文献
Klemmensen,P.D. et al.
Journal of Organic Chemistry, 1979 , vol. 44, # 3 p. 416 - 420
反应条件
1: 79 percent / 3,3',3''-phosphinidynetris-benzenesulfonic acid tri-Na salt; K2CO3 / Pd(OAc)2 / H2O; ethanol / 3 h / 100 °C 2: 42 percent / 3,3',3''-phosphinidynetris-benzenesulfonic acid tri-Na salt / Pd(OAc)2 / H2O; ethanol / 1.5 h / 80 °C View Scheme
参考文献
Yokoyama, Yuusaku; Takagi, Noriko; Hikawa, Hidemasa; Kaneko, Satoru; Tsubaki, Natsume; Okuno, Hiroaki
Advanced Synthesis and Catalysis, 2007 , vol. 349, # 4-5 p. 662 - 668
反应条件
1: 4-(N,N-dimethlyamino)pyridine; triethylamine / dichloromethane 2: C17H25N2OP; potassium carbonate; bis(dibenzylideneacetone)-palladium(0) / dimethyl sulfoxide / 18 h / 20 °C / Inert atmosphere View Scheme
参考文献
Vasil'ev; Lyubimov; Serebryakov; Davankov; Struchkova; Zlotina
Russian Chemical Bulletin, 2010 , vol. 59, # 3 p. 605 - 610
反应条件
mesoporous silica containing bimetallic Cu-Al (CuAl-KIT-5) in 1,2-dichloro-ethane T=60 - 85°C; 7 h;
参考文献
Varghese, Shaji; Anand, Chokkalingam; Dhawale, Dattatray; Mane, Gurudas P.; Wahab, Mohammad A.; Mano, Ajayan; Raj, George Allen Gnana; Nagarajan, Samuthira; Vinu, Ajayan
ChemCatChem, 2013 , vol. 5, # 4 p. 899 - 902
反应条件
boron trifluoride diethyl etherate in 1,4-dioxane Ambient temperature;
参考文献
Ferrari, F.; Monache, G. Delle; Lima, R. Alves
Phytochemistry (Elsevier), 1985 , vol. 24, # 11 p. 2753 - 2755
反应条件
boron trifluoride diethyl etherate in 1,4-dioxane T=20°C; 72 h;
参考文献
Helesbeux, Jean-Jacques; Duval, Olivier; Guilet, David; Seraphin, Denis; Rondeau, David; Richomme, Pascal
Tetrahedron, 2003 , vol. 59, # 27 p. 5091 - 5104
反应条件
sulfuric acid T=25°C;
参考文献
Faworski; Lebedewa
Zhurnal Obshchei Khimii, 1938 , vol. 8, p. 882
Bulletin de la Societe Chimique de France, 1939 , vol. <5>6, p. 1351
Chem. Zentralbl., 1939 , vol. 110, # I p. 4330
Full Text Show Details
Faworski; Lebedewa
Bulletin de la Societe Chimique de France, 1939 , vol. <5>6, p. 1347,1351
