2-甲基-3-丁烯-2-醇合成路线 （共 471 条）
参考文献
Johnston, Blair D.; Czyzewska, Eva; Oehlschlager, Allan C.
Journal of Organic Chemistry, 1987 , vol. 52, # 16 p. 3693 - 3697
反应条件
tetrakis(triphenylphosphine) palladium(0) in dichloromethane
T=80°C; 48 h;
参考文献
Tsukamoto, Hirokazu; Sato, Masanori; Kondo, Yoshinori
Chemical Communications, 2004 , # 10 p. 1200 - 1201
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran
T=80°C; 24 h; Inert atmosphere;
参考文献
Tsukamoto, Hirokazu; Uchiyama, Tomomi; Suzuki, Takamichi; Kondo, Yoshinori
Organic and Biomolecular Chemistry, 2008 , vol. 6, # 16 p. 3005 - 3013
反应条件
toluene-4-sulfonic acid in dichloromethane
4 h; Heating;
参考文献
Ishino; Mihara; Hayakawa; Miyata; Kaneko
Synthetic Communications, 2001 , vol. 31, # 3 p. 439 - 448
反应条件
phosphoric acid
T=20°C; 12 h;
参考文献
Baird, Kenneth J.; Grundon, Michael F.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1820 - 1825
反应条件
1: 16 percent / 5percent aq.citric acid / 0.5 h / Heating
2: 2 h / 200 °C
View Scheme
参考文献
Baird, Kenneth J.; Grundon, Michael F.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1820 - 1825
反应条件
toluene-4-sulfonic acid in dichloromethane
4 h; Heating;
参考文献
Ishino; Mihara; Hayakawa; Miyata; Kaneko
Synthetic Communications, 2001 , vol. 31, # 3 p. 439 - 448
反应条件
citric acid
0.5 h; Heating;
参考文献
Baird, Kenneth J.; Grundon, Michael F.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1820 - 1825
反应条件
1: 25 percent / ortophosphoric acid / 12 h / 20 °C
2: 98 percent / boron trichloride / CH2Cl2 / 2 h / 0 °C
3: n-butyl lithium / diethyl ether / 20 °C
View Scheme
参考文献
Baird, Kenneth J.; Grundon, Michael F.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1820 - 1825
反应条件
1: aqueous H3PO4
2: palladium/CaCO3; ethanol / Hydrogenation
View Scheme
参考文献
Kachniaschwili et al.
Zhurnal Obshchei Khimii, 1955 , vol. 25, p. 117; engl. Ausg. S. 101
