2-甲基-3-丁烯-2-醇合成路线 （共 471 条）
反应条件
sulfuric acid
T=60 - 65°C;
参考文献
Nasarow; Aserbajew; Raktschejewa
Zhurnal Obshchei Khimii, vol. 18, p. 409
Chem.Abstr., 1949 , p. 113
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Nasarow; Aserbajew; Raktschejewa
Zhurnal Obshchei Khimii, 1948 , vol. 18, p. 408,411
Chem.Abstr., 1949 , p. 113
参考文献
Nasarow; Aserbajew; Raktschejewa
Zhurnal Obshchei Khimii, 1948 , vol. 18, p. 408,411
Chem.Abstr., 1949 , p. 113
反应条件
hydrogenchloride in water
0.25 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Laduranty, Joelle; Barbot, Francis; Miginiac, Leone
Bulletin de la Societe Chimique de France, 1989 , # 6 p. 850 - 855
反应条件
hydrogenchloride
T=0°C;
参考文献
Magid,R.M. et al.
Journal of Organic Chemistry, 1979 , vol. 44, # 3 p. 359 - 363
反应条件
1,1,1,3,3,3-hexachloro-propan-2-one; triphenylphosphine in various solvent(s)
1 h; from 10 deg C to room temp., solvent: hexachloroacetone;
参考文献
Magid, Ronald M.; Talley, Brenda G.; Souther, Stephen K.
Journal of Organic Chemistry, 1981 , vol. 46, # 4 p. 824 - 825
参考文献
Nasarow; Aserbajew
Zhurnal Obshchei Khimii, 1948 , vol. 18, p. 419,421
Chem.Abstr., 1949 , p. 114
参考文献
Laforgue
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1948 , vol. 227, p. 353
反应条件
sodium hydride; Cl2Ni(1,2-bis(diphenylphosphino)ethane) in tetrahydrofuran
T=65°C; 36 h; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Alvarez, Eleuterio; Cuvigny, Therese; Julia, Marc
Journal of Organometallic Chemistry, 1988 , vol. 339, p. 199 - 212
反应条件
sodium hydride; Cl2Ni(1,2-bis(diphenylphosphino)ethane) in tetrahydrofuran
T=65°C; 36 h; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Alvarez, Eleuterio; Cuvigny, Therese; Julia, Marc
Journal of Organometallic Chemistry, 1988 , vol. 339, p. 199 - 212
反应条件
1: pyridine / diethyl ether / Heating
2: 1.) NaH, 2.) Bu4N<Fe(CO)3NO> / 1.) THF, 10 min, 2.) THF, reflux, 12 h
View Scheme
参考文献
Xu, Yuanyao; Zhou, Bo
Journal of Organic Chemistry, 1987 , vol. 52, # 6 p. 974 - 977
