2-甲基-3-丁烯-2-醇合成路线 （共 471 条）
反应条件
aluminum isopropoxide
T=220°C;
参考文献
Colonge,J. et al.
Bulletin de la Societe Chimique de France, 1965 , p. 2733 - 2738
反应条件
phosphoric acid
T=150°C; P=3800 Torr; 2 h;
参考文献
Liu, Changqing; Kudo, Kazuaki; Hashimoto, Yukihiko; Saigo, Kazuhiko
Journal of Organic Chemistry, 1996 , vol. 61, # 2 p. 494 - 502
反应条件
phosphoric acid
T=150°C; 4 h; Title compound not separated from byproducts;
参考文献
Jin, Qingwu; Coates, Robert M.
Collection of Czechoslovak Chemical Communications, 2002 , vol. 67, # 1 p. 55 - 74
反应条件
1: (1,10-phenanthroline)palladium(II) acetate / 85 °C
2: 0.5 h / 120 °C
View Scheme
参考文献
Wei, Xudong; Lorenz, Jon C.; Kapadia, Suresh; Saha, Anjan; Haddad, Nizar; Busacca, Carl A.; Senanayake, Chris H.
Journal of Organic Chemistry, 2007 , vol. 72, # 11 p. 4250 - 4253
反应条件
sulfuric acid; copper(II) sulfate
参考文献
Nasarow; Jufit
Zhurnal Obshchei Khimii, 1959 , vol. 29, p. 783,786;engl.Ausg.S.770
反应条件
pyridine in dichloromethane
T=0°C; 15 h;
参考文献
Babin, Didier; Fourneron, Jean-Dominique; Julia, Marc
Bulletin de la Societe Chimique de France, 1980 , vol. 2, # 11-12 p. 588 - 600
反应条件
in chloroform-d1; dichloromethane
T=-15 - 0°C; 60 h; Product distribution;
参考文献
Babin, Didier; Fourneron, Jean-Dominique; Julia, Marc
Bulletin de la Societe Chimique de France, 1980 , vol. 2, # 11-12 p. 588 - 600
反应条件
pyridine in diethyl ether; dichloromethane
T=0°C; 2 h;
参考文献
Babin, Didier; Fourneron, Jean-Dominique; Julia, Marc
Bulletin de la Societe Chimique de France, 1980 , vol. 2, # 11-12 p. 588 - 600
反应条件
in chloroform-d1; dichloromethane
T=-15 - 0°C; 60 h; Product distribution;
参考文献
Babin, Didier; Fourneron, Jean-Dominique; Julia, Marc
Bulletin de la Societe Chimique de France, 1980 , vol. 2, # 11-12 p. 588 - 600
反应条件
1: 18 percent / BF3-etherate / dioxane / 6 h / 51 - 53 °C
2: 50 percent / 4percent aq. NaOH / methanol / 1.5 h / 50 °C
View Scheme
参考文献
Tsukayama, Masao; Fujimoto, Kunihiro; Horie, Tokunaru; Yamashita, Yoshiro; Masumura, Mitsuo; Nakayama, Mitsuru
Chemistry Letters, 1982 , p. 675 - 678
