2-甲基-3-丁烯-2-醇合成路线 (共 471 条)
反应条件
phosphoric acid in Petroleum ether
T=35 - 40°C; 4 h;
参考文献
Ahluwalia, V. K.; Arora, K. K.; Anand, Saroj
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 2 p. 129 - 131
反应条件
triethyl borane; triethylamine; tetrakis(triphenylphosphine) palladium(0) in hexane; toluene
T=50°C; 24 h; Product distribution; Further Variations:Temperatures;
参考文献
Kimura, Masanari; Fukasaka, Miki; Tamaru, Yoshinao
Heterocycles, 2006 , vol. 67, # 2 p. 535 - 542
反应条件
zinc(II) chloride in 1,2-dichloro-ethane
T=20°C; 0.5 h;
参考文献
Clarembeau, M.; Krief, A.
Tetrahedron Letters, 1984 , vol. 25, # 33 p. 3625 - 3628
反应条件
boron trifluoride diethyl etherate in 1,4-dioxane
T=20°C; 5.5 h; Further byproducts given;
参考文献
Cann, Martin R.; Davis, Anne-Marie; Shannon, Patrick V. R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 7 p. 1413 - 1421
反应条件
trifluoroacetic acid
T=20°C; Inert atmosphere;
参考文献
Yang, Jie; Liu, Guo-Yun; Lu, Dong-Liang; Dai, Fang; Qian, Yi-Ping; Jin, Xiao-Ling; Zhou, Bo
Chemistry - A European Journal, 2010 , vol. 16, # 43 p. 12808 - 12813
反应条件
CuAl-SBA-15 in cyclohexane
T=85°C; 16 h;
参考文献
Varghese, Shaji; Anand, Chokkalinkam; Dhawale, Dattatray; Mano, Ajayan; Balasubramanian, Veerappan V.; Raj, George Allen Gnana; Nagarajan, Samuthira; Wahab, Mohammad A.; Vinu, Ajayan
Tetrahedron Letters, 2012 , vol. 53, # 42 p. 5656 - 5659
反应条件
1: petroleum ether; PBr3 / -15 °C
2: zinc chloride
View Scheme
参考文献
Karrer et al.
Helvetica Chimica Acta, 1939 , vol. 22, p. 1287,1290
反应条件
boron trifluoride; zinc(II) chloride
anschliessend Behandeln mit Ag2O;
参考文献
Isler et al.
Hoppe-Seyler's Zeitschrift fuer Physiologische Chemie, 1953 , vol. 295, p. 290,307
Helvetica Chimica Acta, 1958 , vol. 41, p. 786,803
反应条件
phosphoric acid
T=20°C; 12 h;
参考文献
Baird, Kenneth J.; Grundon, Michael F.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1820 - 1825
反应条件
1: hydrogen bromide
2: folgend Behandlung des Reaktionsprodukts mit verd. Salzsaeure
View Scheme
参考文献
Makida, Yusuke; Ohmiya, Hirohisa; Sawamura, Masaya
Chemistry - An Asian Journal, 2011 , vol. 6, # 2 p. 410 - 414