2-甲基-3-丁烯-2-醇合成路线 （共 471 条）
反应条件
trifluoroacetic acid in nitromethane
T=0°C; 1.5 h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Badet,B.; Julia,M.; Mallet,J.M.
Tetrahedron, 1988 , vol. 44, p. 2913
反应条件
1: TFA / nitromethane / 1.5 h / 0 °C
2: POCl3 / pyridine / 15 h / Ambient temperature
View Scheme
参考文献
Badet,B.; Julia,M.; Mallet,J.M.
Tetrahedron, 1988 , vol. 44, p. 2913
反应条件
chlorine in tetrachloromethane
T=5°C;
参考文献
Bentley, Stuart; Goosen, Andre; Laue, Hugh A. H.; Taljaard, Benjamin
Journal of Chemical Research, Miniprint, 1991 , p. 1566 - 1590
反应条件
1: chloroform; chlorine / -10 - -5 °C
2: P2O5 / 98 °C / 100 Torr
View Scheme
参考文献
Petrow
Zhurnal Obshchei Khimii, 1943 , vol. 13, p. 741,748
Zhurnal Obshchei Khimii, 1945 , vol. 15, p. 931,937
Chem.Abstr., 1945 , p. 696,1946 6415
反应条件
boron trifluoride diethyl etherate in 1,4-dioxane
1 h; Ambient temperature;
参考文献
Jain; Prasad
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1990 , vol. 29, # 6 p. 525 - 528
反应条件
boron trifluoride diethyl etherate
参考文献
Collins,E. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1975 , p. 96 - 101
反应条件
trifluoroacetic acid in water
Ambient temperature;
参考文献
Ismail, Fyaz M. D.; Hilton, Mark J.; Stefmovic, Marijan
Tetrahedron Letters, 1992 , vol. 33, # 26 p. 3795 - 3796
反应条件
1: With o-hydroxynitrobenzene
36 h; Heating;
2: With hydrogenchloride in methanol; water
T=20°C; 12 h;
3: With potassium hydroxide in ethanol; water
24 h; Heating; Further stages.;
参考文献
Menon, Suneetha; Sinha-Mahapatra, Dilip; Herndon, James W.
Tetrahedron, 2007 , vol. 63, # 36 p. 8788 - 8793
反应条件
1: AIBN
2: aq. KOH / ethanol
View Scheme
参考文献
Surzur,J.-M.; Teissier,P.
Bulletin de la Societe Chimique de France, 1970 , p. 653 - 664
反应条件
ammonium cerium (IV) nitrate; dihydrogen peroxide; lithium bromide in water
T=65 - 70°C; 5 h; Reagent/catalyst;
参考文献
Nikishin; Sokova; Kapustina
Russian Chemical Bulletin, 2012 , vol. 61, # 2 p. 459 - 463
Izv. Akad. Nauk, Ser. Khim., 2012 , # 2 p. 456 - 460,5
