2-甲基-3-丁烯-2-醇合成路线 (共 471 条)
反应条件
trifluoroacetic acid in dichloromethane
T=0°C; 0.333333 h; reaction with isopentenyl derivatives and their homologs in var. solvents; Product distribution;
参考文献
Badet,B.; Julia,M.; Mallet,J.M.
Tetrahedron, 1988 , vol. 44, p. 2913
反应条件
boron trifluoride diethyl etherate in 1,4-dioxane
T=20°C; 72 h;
参考文献
Helesbeux, Jean-Jacques; Duval, Olivier; Guilet, David; Seraphin, Denis; Rondeau, David; Richomme, Pascal
Tetrahedron, 2003 , vol. 59, # 27 p. 5091 - 5104
反应条件
tricyclo[3.3.1.13,7 ]-decane-1-carboxylic acid; triphenylphosphine; bis(acetylacetonato) palladium in water
0.5 h; Heating;
参考文献
Yang, Shyh-Chyun; Hsu, Yi-Chun; Gan, Kim-Hong
Tetrahedron, 2006 , vol. 62, # 17 p. 3949 - 3958
反应条件
1.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere
1.2: 1 h / 0 °C / Inert atmosphere
2.1: bis(bicyclo[2.2.1]hepta-2,5-diene)dichlorodirhodium / tetrahydrofuran / 0.5 h / 25 °C / Inert atmosphere
View Scheme
参考文献
Arnold, Jeffrey S.; Cizio, Gregory T.; Nguyen, Hien M.
Organic Letters, 2011 , vol. 13, # 20 p. 5576 - 5579
反应条件
potassium hydride in tetrahydrofuran
参考文献
Astin,K.B.; Whiting,M.C.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1976 , p. 1157 - 1160
反应条件
sodium acetate in chloroform
参考文献
BASF Aktiengesellschaft
Patent: US4475003 A1, 1984 ;
反应条件
sodium acetate in chloroform
参考文献
BASF Aktiengesellschaft
Patent: US4475003 A1, 1984 ;
反应条件
sodium acetate; dibenzoyl peroxide in chloroform; water
参考文献
BASF Aktiengesellschaft
Patent: US4475003 A1, 1984 ;
参考文献
BASF Aktiengesellschaft
Patent: US4475003 A1, 1984 ;
反应条件
di-tert-butyl phosphite; dibenzoyl peroxide in cyclohexane
T=80°C;
参考文献
Barks; Gilbert; Parsons; Upeandran
Synlett, 2001 , # 11 p. 1719 - 1722