2-甲基-3-丁烯-2-醇合成路线 （共 471 条）
反应条件
in formic acid; water
T=80°C;
参考文献
Brown, Roger F. C.; Matthews, Barry R.; Rae, Ian D.
Tetrahedron Letters, 1981 , vol. 22, # 30 p. 2915 - 2918
参考文献
Manners,G. et al.
Tetrahedron, 1972 , vol. 28, p. 2949 - 2959
反应条件
sodium hydrogencarbonate; palladium (II) bromide; copper dichloride in dimethyl sulfoxide
T=70°C; Heck reaction; 24 h;
参考文献
Huang, Qinhua; Larock, Richard C.
Tetrahedron Letters, 2002 , vol. 43, # 19 p. 3557 - 3560
反应条件
hydrogen; RhH(CO)(triphenylphosphine)3; dicobalt octacarbonyl in 1,4-dioxane
100 atm, 25 deg C and 120 deg C, 16 h, then 130 atm 2 to 3 h; Yield given. Yields of byproduct given;
参考文献
Yuan, Sun-Shine; Ajami, Alfred M.
Journal of Organometallic Chemistry, 1986 , vol. 302, # 2 p. 255 - 258
反应条件
hydrogen; RhH(CO)(triphenylphosphine)3; dicobalt octacarbonyl in 1,4-dioxane
100 atm, 25 deg C and 120 deg C, 16 h, then 130 atm 2 to 3 h; Yield given. Yields of byproduct given;
参考文献
Yuan, Sun-Shine; Ajami, Alfred M.
Journal of Organometallic Chemistry, 1986 , vol. 302, # 2 p. 255 - 258
反应条件
chloro-trimethyl-silane; water; sodium iodide in acetonitrile
0.5 h; Ambient temperature;
参考文献
Kanai, Takaya; Irifune, Shinji; Ishii, Yasutaka; Ogawa, Masaya
Synthesis, 1989 , # 4 p. 283 - 286
反应条件
diphosphorous tetraiodide
T=85°C; P=0.01 Torr; 0.0833333 h; Title compound not separated from byproducts;
参考文献
Lasne, Marie- Claire; Cairon, Philippe; Villemin, D.
Synthetic Communications, 1990 , vol. 20, # 1 p. 41 - 44
参考文献
Bouchoux, Guy; Hoppilliard, Yannik; Jaudon, Pascale
Organic Mass Spectrometry, 1987 , vol. 22, p. 98 - 102
反应条件
sodium hydride
1. 1 h; 2. overnight; Multistep reaction;
参考文献
Tzeng, Dongjaw; Weber, William P.
Journal of Organic Chemistry, 1981 , vol. 46, # 4 p. 693 - 696
反应条件
sulfuric acid
T=60 - 65°C;
参考文献
Nasarow; Aserbajew; Raktschejewa
Zhurnal Obshchei Khimii, vol. 18, p. 409
Chem.Abstr., 1949 , p. 113
Full Text Show Details
Nasarow; Aserbajew; Raktschejewa
Zhurnal Obshchei Khimii, 1948 , vol. 18, p. 408,411
Chem.Abstr., 1949 , p. 113
