2-甲基-3-丁烯-2-醇合成路线 （共 471 条）
参考文献
Courtot
Bulletin de la Societe Chimique de France, 1906 , vol. <3> 35, p. 660
反应条件
1: BF3*OEt2 / dioxane 2: 56 percent / DDQ / toluene / Heating View Scheme
参考文献
Ho, Li-Kang; Yu, Hsi-Jung; Ho, Chen-Ta; Don, Ming-Jaw
Journal of the Chinese Chemical Society, 2001 , vol. 48, # 1 p. 77 - 79
反应条件
1: 540 mg / BF3*Et2O / dioxane / 2 h / Ambient temperature 2: 160 mg / 2,3-dicyano-5,6-dichloro-p-benzoquinone (DDQ) / diethyl ether / Ambient temperature View Scheme
参考文献
Nomura, Taro; Fukai, Toshio; Hano, Yoshio; Tsukamoto, Koji
Heterocycles, 1983 , vol. 20, # 4 p. 661 - 666
反应条件
trifluoroacetic acid in nitromethane T=0°C; 1.5 h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Badet,B.; Julia,M.; Mallet,J.M.
Tetrahedron, 1988 , vol. 44, p. 2913
反应条件
1: TFA / nitromethane / 1.5 h / 0 °C 2: POCl3 / pyridine / 15 h / Ambient temperature View Scheme
参考文献
Badet,B.; Julia,M.; Mallet,J.M.
Tetrahedron, 1988 , vol. 44, p. 2913
反应条件
hydrogenchloride in water 0.25 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Laduranty, Joelle; Barbot, Francis; Miginiac, Leone
Bulletin de la Societe Chimique de France, 1989 , # 6 p. 850 - 855
反应条件
hydrogenchloride T=0°C; 1 h;
参考文献
Vani; Chida; Srinivasan; Chandrasekharam; Singh
Synthetic Communications, 2001 , vol. 31, # 2 p. 219 - 224
反应条件
in dichloromethane T=20°C; 1 h;
参考文献
Kishali, Nurhan; Polat, M. Fatih; Altundas, Ramazan; Kara, Yunus
Helvetica Chimica Acta, 2008 , vol. 91, # 1 p. 67 - 72
反应条件
1,1,1,3,3,3-hexachloro-propan-2-one; triphenylphosphine in various solvent(s) 1 h; from 10 deg C to room temp., solvent: hexachloroacetone;
参考文献
Magid, Ronald M.; Talley, Brenda G.; Souther, Stephen K.
Journal of Organic Chemistry, 1981 , vol. 46, # 4 p. 824 - 825
参考文献
Nasarow; Aserbajew
Zhurnal Obshchei Khimii, 1948 , vol. 18, p. 419,421
Chem.Abstr., 1949 , p. 114
