2-甲基-3-丁烯-2-醇合成路线 （共 471 条）
参考文献
Laforgue
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1948 , vol. 227, p. 353
反应条件
1: 76 percent / H3PO4 / 2 h / 150 °C / 3800 Torr 2: 74 percent / NaBH4 / H2O / 50 deg C -> 30 deg C View Scheme
参考文献
Yonova, Ivelina M.; Johnson, A. George; Osborne, Charlotte A.; Moore, Curtis E.; Morrissette, Naomi S.; Jarvo, Elizabeth R.
Angewandte Chemie - International Edition, 2014 , vol. 53, # 9 p. 2422 - 2427
Angew. Chem., 2014 , vol. 126, # 9 p. 2454 - 2459,6
参考文献
Schneider; Cloux; Foti; Kovats
Synthesis, 1990 , # 11 p. 1027 - 1031
反应条件
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Schneider; Cloux; Foti; Kovats
Synthesis, 1990 , # 11 p. 1027 - 1031
反应条件
1: With formic acid in tetrahydrofuran 3 h; Reflux; 2: With hydrogenchloride; methanol in water 0.333333 h; Reflux;
参考文献
Kloser, Elisabeth; Boehmdorfer, Stefan; Brecker, Lothar; Kaehlig, Hanspeter; Netscher, Thomas; Mereiter, Kurt; Rosenau, Thomas
European Journal of Organic Chemistry, 2011 , # 13 p. 2450 - 2457
反应条件
toluene-4-sulfonic acid in toluene T=100°C; 18 h;
参考文献
Hong, Mei Peng; Webster, Richard D.
Journal of Organic Chemistry, 2008 , vol. 73, # 6 p. 2169 - 2175
反应条件
1: 1,1-dimethylallyl alcohol With hydrogenchloride T=-5 - 0°C; 1.5 h; 2: With magnesium in tetrahydrofuran 5.3 h; 3: carbon dioxide 2 h; Title compound not separated from byproducts;
参考文献
Fekner, Tomasz; Mueller-Bunz, Helge; Guiry, Patrick J.
Organic Letters, 2006 , vol. 8, # 22 p. 5109 - 5112
反应条件
in pentane Irradiation; Product distribution;
参考文献
Tetrahedron Letters, , vol. 36, # 19 p. 3315 - 3316
反应条件
palladium diacetate; triethylamine T=120 - 130°C; 1 h; effect of temperature; Product distribution;
参考文献
Somei; Yamada
Chemical and Pharmaceutical Bulletin, 1984 , vol. 32, # 12 p. 5064 - 5065
反应条件
in paraffin 1.) 160 deg C, 6 h, 2.) 180 deg C, 3 h;
参考文献
Sobenina; Mikhaleva; Petrova; Polovnikova; Trofimov
Russian Journal of Organic Chemistry, 1997 , vol. 33, # 7 p. 1041 - 1042
